cyanomethyl 2-acetamido-2-deoxy-1-*thio-B-D-gluco

Base Information

Chemical Name:cyanomethyl 2-acetamido-2-deoxy-1-*thio-B-D-gluco
CAS No.:61145-38-8
Molecular Formula:
Molecular Weight:276.31
Hs Code.:

Synonyms:CYANOMETHYL 2-ACETAMIDO-2-DEOXY-1-THIO-B -D-GLUCOPY;cyanomethyl 2-acetamido-2-deoxy-1-*thio-B-D-gluco;CYANOMETHYL 2-ACETAMIDO-2-DEOXY-1-THIO-B-D-GLUCOPYRANOSIDE;cyanomethylacetamido-2-deoxy-1-thio-beta-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyanomethyl 2-acetamido-2-deoxy-1-*thio-B-D-gluco

Chemical Property:

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Technology Process of cyanomethyl 2-acetamido-2-deoxy-1-*thio-B-D-gluco

There total 6 articles about cyanomethyl 2-acetamido-2-deoxy-1-*thio-B-D-gluco which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 61145-37-7
2-N-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio(S-cyanomethyl)-β-D-glucopyranoside

: 61145-38-8
S-cyanomethyl 2-N-acetamido-2-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: With methanol; triethylamine; at 20 ℃; for 24h;

Reference yield:

: 61145-37-7
2-N-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio(S-cyanomethyl)-β-D-glucopyranoside

: 124-41-4
sodium methylate

: 75204-31-8
2-acetamido-1-thio-(S-2-imido-2-methoxyethyl)-2-deoxy-β-D-glucopyranoside

: 61145-38-8
S-cyanomethyl 2-N-acetamido-2-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: In methanol; at 20 ℃; for 16h;
DOI:10.1016/j.ica.2019.05.032

Reference yield:

: 51224-18-1
S-thiouronium 2-N-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside hydrochloride

: 61145-38-8
S-cyanomethyl 2-N-acetamido-2-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; sodium metabisulfite / acetone; water / 16 h / 25 °C

2: triethylamine; methanol / 24 h / 20 °C

With methanol; sodium metabisulfite; potassium carbonate; triethylamine; In water; acetone;