1-(1,2,3,4-Tetrahydroisoquinolin-7-yl)ethanone hydrochloride

Base Information

Chemical Name:1-(1,2,3,4-Tetrahydroisoquinolin-7-yl)ethanone hydrochloride
CAS No.:82771-27-5
Molecular Formula:C₁₁H₁₃NO*ClH
Molecular Weight:211.691
Hs Code.:2933499090
DSSTox Substance ID:DTXSID20510737
Mol file:82771-27-5.mol

Synonyms:82771-27-5;1-(1,2,3,4-Tetrahydroisoquinolin-7-yl)ethanone hydrochloride;1-(1,2,3,4-tetrahydroisoquinolin-7-yl)ethan-1-one hydrochloride;1-(1,2,3,4-tetrahydroisoquinolin-7-yl)ethanone;hydrochloride;DTXSID20510737;1-(1,2,3,4-Tetrahydroisoquinolin-7-yl)ethanonehydrochloride;AKOS016001790;CS-0363287;F10170;A864346;1-(1,2,3,4-Tetrahydroisoquinolin-7-yl)ethan-1-one--hydrogen chloride (1/1)

Suppliers and Price of 1-(1,2,3,4-Tetrahydroisoquinolin-7-yl)ethanone hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1-(1,2,3,4-Tetrahydroisoquinolin-7-yl)ethanonehydrochloride 95+%
1g
$ 535.00

Chemenu
1-(1,2,3,4-tetrahydroisoquinolin-7-yl)ethan-1-onehydrochloride 95%
1g
$ 505.00

American Custom Chemicals Corporation
1-(1,2,3,4-TETRAHYDROISOQUINOLIN-7-YL)ETHANONE HYDROCHLORIDE 95.00%
5MG
$ 495.13

Alichem
1-(1,2,3,4-Tetrahydroisoquinolin-7-yl)ethanonehydrochloride
1g
$ 466.52

Total 10 raw suppliers

Chemical Property of 1-(1,2,3,4-Tetrahydroisoquinolin-7-yl)ethanone hydrochloride

Chemical Property:

Melting Point:230-231 °C(Solv: ethanol (64-17-5))
PSA：29.10000
LogP:2.66570
Storage Temp.:Sealed in dry,Room Temperature
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:211.0763918
Heavy Atom Count:14
Complexity:202

Purity/Quality:

97% ^*data from raw suppliers

1-(1,2,3,4-Tetrahydroisoquinolin-7-yl)ethanonehydrochloride 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)C1=CC2=C(CCNC2)C=C1.Cl

Technology Process of 1-(1,2,3,4-Tetrahydroisoquinolin-7-yl)ethanone hydrochloride

There total 4 articles about 1-(1,2,3,4-Tetrahydroisoquinolin-7-yl)ethanone hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 82771-26-4
7-acetyl-2-(trifluoroacetyl)-1,2,3,4-tetrahydroisoquinoline

: 82771-27-5
7-acetyl-1,2,3,4-tetrahydroisoquinoline hydrochloride

Guidance literature:: With hydrogenchloride; In butan-1-ol; for 3h; Heating;
DOI:10.1021/jm00352a028

Reference yield:

: 91-21-4
1,2,3,4-tetrahydroisoquinoline

: 82771-27-5
7-acetyl-1,2,3,4-tetrahydroisoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / 16 h / 25 °C

2: 66 percent / AlCl₃ / CS₂ / 1 h / Heating

3: 83 percent / 3N aq. HCl / butan-1-ol / 3 h / Heating

With hydrogenchloride; aluminium trichloride; In carbon disulfide; butan-1-ol;
DOI:10.1021/jm00352a028

Reference yield:

: 55649-51-9
2-(trifluoroacetyl)-1,2,3,4-tetrahydroisoquinoline

: 82771-27-5
7-acetyl-1,2,3,4-tetrahydroisoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / AlCl₃ / CS₂ / 1 h / Heating

2: 83 percent / 3N aq. HCl / butan-1-ol / 3 h / Heating

With hydrogenchloride; aluminium trichloride; In carbon disulfide; butan-1-ol;
DOI:10.1021/jm00352a028