N-Propyl L-Z-ValinaMide

Base Information

Chemical Name:N-Propyl L-Z-ValinaMide
CAS No.:861904-21-4
Molecular Formula:C8H18N2O
Molecular Weight:292.378
Hs Code.:

Synonyms:N-Propyl L-Z-ValinaMide

Suppliers and Price of N-Propyl L-Z-ValinaMide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N-Propyl L-Z-ValinaMide

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-Propyl L-Z-ValinaMide

There total 6 articles about N-Propyl L-Z-ValinaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 107-10-8,42939-71-9
propylamine

: 1149-26-4
(S)-N-(benzyloxycarbonyl)valine

: 861904-21-4
(S)-benzyl (3-methyl-1-oxo-1-(propylamino)butan-2-yl)carbamate

Guidance literature:: (S)-N-(benzyloxycarbonyl)valine; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

propylamine; In tetrahydrofuran; at 0 - 20 ℃; for 12.25h; Inert atmosphere;
DOI:10.1016/j.bmcl.2018.02.005

Reference yield: 95.0%

: 107-10-8,42939-71-9
propylamine

: 3496-11-5
2,5-dioxopyrrolidin-1-yl (2S)-2-(((benzyloxy)carbonyl)amino)-3-methylbutanoate

: 861904-21-4
(S)-benzyl (3-methyl-1-oxo-1-(propylamino)butan-2-yl)carbamate

Guidance literature:: In tetrahydrofuran; for 4h; Heating;
DOI:10.1016/j.tet.2007.06.087

Reference yield:

: 1149-26-4
(S)-N-(benzyloxycarbonyl)valine

: 861904-21-4
(S)-benzyl (3-methyl-1-oxo-1-(propylamino)butan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: DCC / tetrahydrofuran / 0 - 5 °C

2: 95 percent / tetrahydrofuran / 4 h / Heating

With dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1016/j.tet.2007.06.087