Ethanol, 2-((6,6-dimethylbicyclo(3.1.1)hept-2-en-2-yl)methoxy)-(9CI)

Base Information

Chemical Name:Ethanol, 2-((6,6-dimethylbicyclo(3.1.1)hept-2-en-2-yl)methoxy)-(9CI)
CAS No.:17140-74-8
Molecular Formula:C₁₂H₂₀O₂
Molecular Weight:196.29
Hs Code.:
DSSTox Substance ID:DTXSID20937985
Mol file:17140-74-8.mol

Synonyms:17140-74-8;2-[(6,6-dimethyl-2-bicyclo[3.1.1]hept-2-enyl)methoxy]ethanol;Ethanol, 2-((6,6-dimethylbicyclo(3.1.1)hept-2-en-2-yl)methoxy)-(9CI);Ethanol, 2-((6,6-dimethylbicyclo(3.1.1)hept-2-en-2-yl)methoxy)-;Ethanol, 2-[(6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)methoxy]-;SCHEMBL15798293;DTXSID20937985;PGPOWYAOSYMYPB-UHFFFAOYSA-N;Ethanol, 2-(2-pinen-10-yloxy)-;2-[(6,6-Dimethylbicyclo[3.1.1]hept-2-en-2-yl)methoxy]ethan-1-ol;2-[(7,7-DIMETHYL-4-BICYCLO[3.1.1]HEPT-3-ENYL)METHOXY]ETHANOL;Ethanol, 2-((6,6-dimethylbicyclo(3.1.1)hept-2-en-2-yl)methoxy)- (9CI)

Suppliers and Price of Ethanol, 2-((6,6-dimethylbicyclo(3.1.1)hept-2-en-2-yl)methoxy)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Ethanol, 2-((6,6-dimethylbicyclo(3.1.1)hept-2-en-2-yl)methoxy)-(9CI)

Chemical Property:

Vapor Pressure:0.000413mmHg at 25°C
Boiling Point:281.8°Cat760mmHg
PKA:14.39±0.10(Predicted)
Flash Point:109.8°C
PSA：29.46000
Density:1.017g/cm³
LogP:1.98770
XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:196.146329876
Heavy Atom Count:14
Complexity:243

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C2CC=C(C1C2)COCCO)C

Technology Process of Ethanol, 2-((6,6-dimethylbicyclo(3.1.1)hept-2-en-2-yl)methoxy)-(9CI)

There total 2 articles about Ethanol, 2-((6,6-dimethylbicyclo(3.1.1)hept-2-en-2-yl)methoxy)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 55527-89-4
(-)-myrtenyl bromide

: 107-21-1
ethylene glycol

: 1337-11-7,17140-74-8
6,6-Dimethyl-2-(2-hydroxyethoxymethyl)bicyclo[3.1.1]hept-2-ene

Guidance literature:: With sodium; In tetrahydrofuran; 1.) reflux, overnight, 2.) reflux, 10 h;
DOI:10.1039/a802024h

Reference yield:

: 18172-67-3,19902-08-0,25719-60-2
beta-pinene

: 1337-11-7,17140-74-8
6,6-Dimethyl-2-(2-hydroxyethoxymethyl)bicyclo[3.1.1]hept-2-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / NBS, dibenzyl peroxide / CCl₄ / 4 h / Heating

2: 99 percent / Na / tetrahydrofuran / 1.) reflux, overnight, 2.) reflux, 10 h

With N-Bromosuccinimide; sodium; benzyl peroxide; In tetrahydrofuran; tetrachloromethane;
DOI:10.1039/a802024h