alpha-(p-Bromobenzyl)-2-thenylamine hydrochloride

Base Information

• Chemical Name: alpha-(p-Bromobenzyl)-2-thenylamine hydrochloride
• CAS No.: 80154-75-2
• Molecular Formula: C₁₂H₁₂BrNS*ClH
• Molecular Weight: 318.665
• DSSTox Substance ID: DTXSID701001018

Synonyms:alpha-(p-Bromobenzyl)-2-thenylamine hydrochloride;2-Thenylamine, alpha-(p-bromobenzyl)-, hydrochloride;80154-75-2;C12H12BrNS.ClH;C12-H12-Br-N-S.Cl-H;DTXSID701001018;LS-149321;2-(4-Bromophenyl)-1-(thiophen-2-yl)ethan-1-amine--hydrogen chloride (1/1)

Chemical Property of alpha-(p-Bromobenzyl)-2-thenylamine hydrochloride

Chemical Property:

• Vapor Pressure: 1.74E-05mmHg at 25°C
• Boiling Point: 363.9°Cat760mmHg
• Flash Point: 173.9°C
• Density: g/cm³
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 316.96406
• Heavy Atom Count: 16
• Complexity: 192

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CSC(=C1)C(CC2=CC=C(C=C2)Br)N.Cl

Technology Process of alpha-(p-Bromobenzyl)-2-thenylamine hydrochloride

There total 1 articles about alpha-(p-Bromobenzyl)-2-thenylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

2-(4-Bromo-phenyl)-1-thiophen-2-yl-ethanone → 2-(4-Bromo-phenyl)-1-thiophen-2-yl-ethylamine; hydrochloride (80154-75-2)

Guidance literature:

With formic acid; ammonium carbonate;

Reference yield: 74.0%

acetic anhydride (108-24-7) + 2-(4-Bromo-phenyl)-1-thiophen-2-yl-ethylamine; hydrochloride (80154-75-2) → N-[2-(4-Bromo-phenyl)-1-thiophen-2-yl-ethyl]-acetamide (80154-77-4)

Guidance literature:

Reference yield:

2-(4-Bromo-phenyl)-1-thiophen-2-yl-ethylamine; hydrochloride (80154-75-2) + acetone (67-64-1) → [2-(4-Bromo-phenyl)-1-thiophen-2-yl-ethyl]-isopropyl-amine; hydrochloride (80154-76-3)

Guidance literature:

With sodium tetrahydroborate; Yield given. Multistep reaction; 1.) reflux, 2.5 h, 2.) MeOH;

Downstream raw materials:

N-[2-(4-Bromo-phenyl)-1-thiophen-2-yl-ethyl]-acetamide

[2-(4-Bromo-phenyl)-1-thiophen-2-yl-ethyl]-isopropyl-amine; hydrochloride

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