2-PHENYL-CYCLOPROPANECARBOXYLIC ACID HYDRAZIDE

Base Information

• Chemical Name: 2-PHENYL-CYCLOPROPANECARBOXYLIC ACID HYDRAZIDE
• CAS No.: 14814-55-2
• Molecular Formula: C10H12N2O
• Molecular Weight: 176.22
• Mol file: 14814-55-2.mol

Synonyms:AKOS B000956;2-PHENYL-CYCLOPROPANECARBOXYLIC ACID HYDRAZIDE;ART-CHEM-BB B000956;2-Phenylcyclopropanecarbohydrazide;2-phenyl-1-cyclopropanecarbohydrazide;2-phenylcyclopropane-1-carbohydrazide;ARONIS020219;MLS000569527

Chemical Property of 2-PHENYL-CYCLOPROPANECARBOXYLIC ACID HYDRAZIDE

Chemical Property:

• PSA: 55.12000
• LogP: 1.87120

Purity/Quality:

97% ^*data from raw suppliers

2-phenylcyclopropanecarbohydrazide ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-PHENYL-CYCLOPROPANECARBOXYLIC ACID HYDRAZIDE

There total 7 articles about 2-PHENYL-CYCLOPROPANECARBOXYLIC ACID HYDRAZIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

methyl 2-phenylcyclopropane-1-carboxylate (20030-70-0) → 2-phenylcyclopropane-1-carbohydrazide (14814-55-2)

Guidance literature:

With hydrazine hydrate; In methanol; at 20 ℃;

DOI:10.1002/cmdc.201900730

Reference yield:

trans-2-phenylcyclopropane-1-carboxylic acid (939-90-2) → 2-phenyl-cyclopropanecarboxylic acid hydrazide (14561-40-1,14814-55-2,17364-52-2)

Guidance literature:

Multistep reaction; (i) CH₂N₂, (ii) N₂H₄*H₂O;

DOI:10.1021/jo01082a600

Reference yield:

cis-methyl 2-phenylcyclopropane-1-carboxylate (67528-62-5) → (+/-)-cis-2-phenyl-cyclopropane-carboxylic acid-(1)-hydrazide (14561-40-1,14814-55-2,17364-52-2)

Guidance literature:

With ethanol; hydrazine hydrate;

DOI:10.1021/ja01186a062

upstream raw materials:

methyl 2-phenylcyclopropane-1-carboxylate

cis-methyl 2-phenylcyclopropane-1-carboxylate

(1S*,2R*)-2-phenylcyclopropane-1-carboxylic acid

methyl trans-2-phenylcyclopropanecarboxylate

Downstream raw materials:

rac-cis-2-phenylcyclopropan-1-amine

(+/-)-cis-2-phenyl-cyclopropane-carboxylic acid-⁽¹⁾-isopropylidenehydrazide

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