10-Methylacridinium chloride

Base Information

• Chemical Name: 10-Methylacridinium chloride
• CAS No.: 5776-39-6
• Molecular Formula: C14H12 N . Cl
• Molecular Weight: 229.709
• DSSTox Substance ID: DTXSID40973345
• Mol file: 5776-39-6.mol

Synonyms:10-Methylacridinium chloride;N-Methylacridinium chloride;5776-39-6;CCRIS 2111;10-methylacridin-10-ium chloride;ACRIDINIUM, 10-METHYL-, CHLORIDE;C14H12N.Cl;SCHEMBL11211685;DTXSID40973345

Chemical Property of 10-Methylacridinium chloride

Chemical Property:

• Melting Point: 122 °C (decomp)
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 3.88000
• Density: g/cm³
• LogP: -0.17850
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 229.0658271
• Heavy Atom Count: 16
• Complexity: 203

Purity/Quality:

10-METHYLACRIDINIUMCHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[N+]1=C2C=CC=CC2=CC3=CC=CC=C31.[Cl-]

Technology Process of 10-Methylacridinium chloride

There total 2 articles about 10-Methylacridinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9,10-dihydro-10-methylacridine (4217-54-3) + benzoic acid-(2,4,6,N-tetrachloro-anilide) (99586-19-3) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 10-methyl-9, 10-dihydro-9-acridinone (719-54-0) + 10-methylacridinium chloride (5776-39-6)

Guidance literature:

Reference yield:

N-methylacridinium iodide (948-43-6) → 10-methylacridinium chloride (5776-39-6)

Guidance literature:

With Dowex-1-X₈ ion exchange coloumn; In water;

DOI:10.1246/bcsj.60.1041

Reference yield: 93.0%

10-methylacridinium chloride (5776-39-6) → 10-methyl-9, 10-dihydro-9-acridinone (719-54-0)

Guidance literature:

With potassium tert-butylate; oxygen; In dimethyl sulfoxide; Ambient temperature;

upstream raw materials:

9,10-dihydro-10-methylacridine

benzoic acid-(2,4,6,N-tetrachloro-anilide)

benzene

N-methylacridinium iodide

Downstream raw materials:

2,2-bis-(10-methyl-9,10-dihydro-acridin-9-yl)-1-phenyl-ethanone

9,10-dihydro-10-methylacridine

10-methyl-9, 10-dihydro-9-acridinone

9-<4-(dimethylamino)phenyl>-10-methylacridinium chloride