4H-Thieno[3,2-b]pyrrole-5-methanol

Base Information

Chemical Name:4H-Thieno[3,2-b]pyrrole-5-methanol
CAS No.:878657-01-3
Molecular Formula:C₇H₇NOS
Molecular Weight:153.205
Hs Code.:
Mol file:878657-01-3.mol

Synonyms:4H-Thieno[3,2-b]pyrrole-5-methanol;(4H-thieno[3,2-b]pyrrol-5-yl)methanol

Suppliers and Price of 4H-Thieno[3,2-b]pyrrole-5-methanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4H-thieno[3,2-b]pyrrol-5-ylmethanol
5mg
$ 45.00

American Custom Chemicals Corporation
(4H-THIENO[3,2-B]PYRROL-5-YL)METHANOL 95.00%
5MG
$ 498.69

Total 1 raw suppliers

Chemical Property of 4H-Thieno[3,2-b]pyrrole-5-methanol

Chemical Property:

PSA：64.26000
LogP:1.72170

Purity/Quality:: 4H-thieno[3,2-b]pyrrol-5-ylmethanol ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4H-Thieno[3,2-b]pyrrole-5-methanol

There total 3 articles about 4H-Thieno[3,2-b]pyrrole-5-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 46193-76-4
ethyl 4H-thieno[3,2-b]pyrrole-5-carboxylate

: 878657-01-3
(4H-thieno[3,2-b]pyrrol-5-yl)methanol

Guidance literature:: ethyl 4H-thieno[3,2-b]pyrrole-5-carboxylate; With lithium aluminium tetrahydride; In tetrahydrofuran; Inert atmosphere;

With water; sodium hydroxide; In tetrahydrofuran;

Reference yield:

: 98-03-3
thiophene-2-carbaldehyde

: 878657-01-3
(4H-thieno[3,2-b]pyrrol-5-yl)methanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium ethanolate / ethanol / 4 h / -10 - 20 °C / Inert atmosphere

1.2: 1 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium ethanolate; In tetrahydrofuran; ethanol;
DOI:10.1016/j.tet.2012.09.011

Reference yield:

: 39793-31-2
4H-thieno[3,2-b]pyrrole-5-carboxylic acid

: 878657-01-3
(4H-thieno[3,2-b]pyrrol-5-yl)methanol

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / Inert atmosphere; Cooling with ice; Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere

With lithium aluminium tetrahydride; thionyl chloride; In tetrahydrofuran;