6-Chloro-5-iodo-3-nitropyridin-2-amine

Base Information

• Chemical Name: 6-Chloro-5-iodo-3-nitropyridin-2-amine
• CAS No.: 790692-90-9
• Molecular Formula: C5H3ClIN3O2
• Molecular Weight: 299.455
• Mol file: 790692-90-9.mol

Synonyms:6-Chloro-5-iodo-3-nitropyridin-2-amine;6-Chloro-5-iodo-3-nitro-pyridin-2-ylamine

Chemical Property of 6-Chloro-5-iodo-3-nitropyridin-2-amine

Chemical Property:

• PSA: 84.73000
• LogP: 2.93440
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

97% ^*data from raw suppliers

6-Chloro-5-iodo-3-nitropyridin-2-amine 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-Chloro-5-iodo-3-nitropyridin-2-amine

There total 1 articles about 6-Chloro-5-iodo-3-nitropyridin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2-amino-6-chloro-3-nitropyridine (27048-04-0) → 6-chloro-5-iodo-3-nitropyridin-2-amine (790692-90-9)

Guidance literature:

With iodine; silver sulfate; In ethanol; at 20 ℃;

Reference yield: 63.0%

((2R,3S)-3-(tert-butyldiphenylsilyloxy)-2,3-dihydrofuran-2-yl)methanol (130277-32-6) + 6-chloro-5-iodo-3-nitropyridin-2-amine (790692-90-9) → C26H28ClN3O5Si

Guidance literature:

6-chloro-5-iodo-3-nitropyridin-2-amine; With triphenyl-arsane; palladium diacetate; In chloroform; at 20 ℃; for 0.5h;

((2R,3S)-3-(tert-butyldiphenylsilyloxy)-2,3-dihydrofuran-2-yl)methanol; With silver carbonate; In chloroform; Reflux;

Reference yield:

6-chloro-5-iodo-3-nitropyridin-2-amine (790692-90-9) → 6-chloro-5-(2,3-dichlorophenyl)pyridine-2,3-diamine (1473416-56-6)

Guidance literature:

Multi-step reaction with 2 steps

1: iron; ammonium chloride / water; ethanol / 4 h / Reflux

2: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; iron; sodium carbonate; ammonium chloride; In 1,4-dioxane; ethanol; water;

upstream raw materials:

2-amino-6-chloro-3-nitropyridine

Downstream raw materials:

6-chloro-5-(2,3-dichlorophenyl)pyridine-2,3-diamine

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