2-Azido-2-deoxy-3-O,4-O-dibenzyl-6-O-acetyl-α-D-glucopyranosyl bromide

Base Information Edit

Chemical Name:2-Azido-2-deoxy-3-O,4-O-dibenzyl-6-O-acetyl-α-D-glucopyranosyl bromide
CAS No.:55682-50-3
Molecular Formula:C₂₂H₂₄BrN₃O₅
Molecular Weight:490.354
Hs Code.:
Mol file:55682-50-3.mol

Synonyms:2-Azido-2-deoxy-3-O,4-O-dibenzyl-6-O-acetyl-α-D-glucopyranosyl bromide

Suppliers and Price of 2-Azido-2-deoxy-3-O,4-O-dibenzyl-6-O-acetyl-α-D-glucopyranosyl bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Azido-2-deoxy-3-O,4-O-dibenzyl-6-O-acetyl-α-D-glucopyranosyl bromide Edit

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Technology Process of 2-Azido-2-deoxy-3-O,4-O-dibenzyl-6-O-acetyl-α-D-glucopyranosyl bromide

There total 9 articles about 2-Azido-2-deoxy-3-O,4-O-dibenzyl-6-O-acetyl-α-D-glucopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 136172-58-2
1,6-di-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α,β-D-glucopyranose

: 55682-50-3
6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl bromide

Guidance literature:: With hydrogen bromide; In acetic acid; for 3.5h;
DOI:10.1016/j.tetasy.2004.11.053

Reference yield:

: 55682-48-9
1,6-anhydro-2-azido-3,4-di-O-benzyl-2-deoxy-D-glucopyranose

: 55682-50-3
6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / 20 °C / Inert atmosphere

2: titanium(IV) bromide / dichloromethane; ethyl acetate / 16 h / 20 °C / Inert atmosphere

With titanium(IV) bromide; trifluoroacetic acid; In dichloromethane; ethyl acetate;