(R)-1-(3-CHLOROPHENYL)ETHANAMINE-HCl

Base Information

• Chemical Name: (R)-1-(3-CHLOROPHENYL)ETHANAMINE-HCl
• CAS No.: 1167414-90-5
• Molecular Formula: C8H11Cl2N
• Molecular Weight: 192.088
• Mol file: 1167414-90-5.mol

Synonyms:(R)-1-(3-CHLOROPHENYL)ETHANAMINE-HCl;(R)-1-(3-Chlorophenyl)ethanaMine hydrochloride

Chemical Property of (R)-1-(3-CHLOROPHENYL)ETHANAMINE-HCl

Chemical Property:

• PSA: 26.02000
• LogP: 3.86200
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

(R)-1-(3-Chlorophenyl)ethanaminehydrochloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (R)-1-(3-CHLOROPHENYL)ETHANAMINE-HCl

There total 2 articles about (R)-1-(3-CHLOROPHENYL)ETHANAMINE-HCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

→ (R)-(+)-1-(3-chlorophenyl)ethylamine hydrochloride (1167414-90-5)

Guidance literature:

Reference yield:

C8H8ClN*ClH (1164111-46-9) → (R)-(+)-1-(3-chlorophenyl)ethylamine hydrochloride (1167414-90-5) + (S)-1-(3-chlorophenyl)ethanamine hydrochloride (1213318-20-7)

Guidance literature:

With chloro(1,5-cyclooctadiene)rhodium(I) dimer; zhaophos; hydrogen; In isopropyl alcohol; at 25 ℃; for 24h; under 7600.51 Torr; Overall yield = 88%; enantioselective reaction; Inert atmosphere; Glovebox; Autoclave;

DOI:10.1002/anie.201404570

Reference yield: 24.0%

(R)-(+)-1-(3-chlorophenyl)ethylamine hydrochloride (1167414-90-5) + ethyl 2-[4-[(1R)-3-oxocyclopentyl]phenyl]acetate (1379647-52-5) → (4-{(1R,3S)-3-[(1R)-1-(3-chloro-phenyl)-ethylamino]-cyclopentyl}-phenyl)-acetic acid ethyl ester (1379647-55-8)

Guidance literature:

With NaBH(OAc)3; In acetonitrile; at 20 ℃;

upstream raw materials:

C₈H₈ClN*ClH

Downstream raw materials:

(4-{(1R,3S)-3-[(1R)-1-(3-chloro-phenyl)-ethylamino]-cyclopentyl}-phenyl)-acetic acid ethyl ester

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