Technology Process of tert-butyl 2-hydroxyphenethylcarbamate
There total 4 articles about tert-butyl 2-hydroxyphenethylcarbamate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 0 ℃;
Inert atmosphere;
DOI:10.1021/jm2007062
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 - 20 °C / Inert atmosphere
2: palladium 10% on activated carbon; hydrogen / ethanol / 20 °C / Inert atmosphere
3: triethylamine / dichloromethane / 0 °C / Inert atmosphere
With
sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; triethylamine;
In
tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1021/jm2007062
- Guidance literature:
-
Multi-step reaction with 4 steps
1: ammonium acetate; acetic acid / 4.5 h / 110 °C / Inert atmosphere
2: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 - 20 °C / Inert atmosphere
3: palladium 10% on activated carbon; hydrogen / ethanol / 20 °C / Inert atmosphere
4: triethylamine / dichloromethane / 0 °C / Inert atmosphere
With
sodium tetrahydroborate; palladium 10% on activated carbon; ammonium acetate; hydrogen; acetic acid; triethylamine;
In
tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1021/jm2007062
