2,4-Dimethylaniline hydrochloride

Base Information

• Chemical Name: 2,4-Dimethylaniline hydrochloride
• CAS No.: 21436-96-4
• Molecular Formula: C8H12ClN
• Molecular Weight: 157.643
• Hs Code.: 2921430090
• European Community (EC) Number: 678-348-3
• UNII: UXP5MZM9MN
• DSSTox Substance ID: DTXSID2021448
• Wikidata: Q27291321
• ChEMBL ID: CHEMBL3186434
• Mol file: 21436-96-4.mol

Synonyms:2,4-dimethylaniline;2,4-xylidine;2,4-xylidine hydrochloride

Chemical Property of 2,4-Dimethylaniline hydrochloride

Chemical Property:

• Vapor Pressure: 0.154mmHg at 25°C
• Melting Point: 238 °C
• Boiling Point: 214.7 °C at 760 mmHg
• Flash Point: 90.6 °C
• PSA: 26.02000
• Density: 0.869g/cm3
• LogP: 3.26880
• Storage Temp.: Inert atmosphere,Room Temperature
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 157.0658271
• Heavy Atom Count: 10
• Complexity: 90.6

Purity/Quality:

98%,99%, ^*data from raw suppliers

2,4-Dimethylaniline Hydrochloride >98.0%(HPLC)(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=C(C=C1)N)C.Cl

Technology Process of 2,4-Dimethylaniline hydrochloride

There total 2 articles about 2,4-Dimethylaniline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-Xylidine (95-68-1) → 2,4-xylidine hydrochloride (21436-96-4)

Guidance literature:

With hydrogenchloride; In water;

DOI:10.1007/s00706-008-0913-5

Reference yield:

→ 2,4-xylidine hydrochloride (21436-96-4)

Guidance literature:

Reference yield: 91.0%

2,4-xylidine hydrochloride (21436-96-4) + formamide (77287-34-4,77287-35-5,60100-09-6) → N-(2,4-dimethylphenyl)formamide (60397-77-5)

Guidance literature:

In toluene; at 120 ℃; for 3h; Green chemistry;

DOI:10.1002/ejoc.202101114

upstream raw materials:

2,4-Xylidine

Downstream raw materials:

2,4,6-trimethylaniline

1-(2,4-xylyl)guanidine

(2,4-dimethylphenyl)thiourea

4,6,8-trimethylquinoline

Refernces

• 1、 Sun, Chuan-Wen,Wang, Hai-Feng,Zhu, Jun,Yang, Ding-Rong,Jin, Jia,Xing, Jia-Hua. "Synthesis, insecticidal activities, and molecular docking studies of 1,5-disubstituted-1,3,5-hexahydrotriazine-2-(N-nitro)imines". experimental part. p. 829 - 835. Retrieved 2011/09/16.
• 2、 -. "Triazapentadienes as acaricides and insecticides". . . Retrieved 2008/06/13.