4-[N-[1,1'-biphenyl]-4-yl-N-9,9-diMethyl-9H-Fluoren-2-aMine]phenylboricacidpinacol ester

Base Information

Chemical Name:4-[N-[1,1'-biphenyl]-4-yl-N-9,9-diMethyl-9H-Fluoren-2-aMine]phenylboricacidpinacol ester
CAS No.:1347758-80-8
Molecular Formula:C39H38BNO2
Molecular Weight:563.54
Hs Code.:
Mol file:1347758-80-8.mol

Synonyms:4-[N-[1,1'-biphenyl]-4-yl-N-9,9-diMethyl-9H-Fluoren-2-aMine]phenylboricacidpinacol ester

Suppliers and Price of 4-[N-[1,1'-biphenyl]-4-yl-N-9,9-diMethyl-9H-Fluoren-2-aMine]phenylboricacidpinacol ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 20 raw suppliers

Chemical Property of 4-[N-[1,1'-biphenyl]-4-yl-N-9,9-diMethyl-9H-Fluoren-2-aMine]phenylboricacidpinacol ester

Chemical Property:

Boiling Point:707.6±60.0 °C(Predicted)
PKA:-3.26±0.40(Predicted)
PSA：21.70000
Density:1.18±0.1 g/cm3(Predicted)
LogP:9.42890

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-[N-[1,1'-biphenyl]-4-yl-N-9,9-diMethyl-9H-Fluoren-2-aMine]phenylboricacidpinacol ester

There total 11 articles about 4-[N-[1,1'-biphenyl]-4-yl-N-9,9-diMethyl-9H-Fluoren-2-aMine]phenylboricacidpinacol ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1246562-40-2
biphenyl-4-yl-(9,9-dimethyl-9H-fluoren-2-yl)-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenylamine

: 73183-34-3
bis(pinacol)diborane

: 1347758-80-8
(N-[1,1‘-biphenyl]-4-yl)-9,9-dimethyl-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)phenyl)-9H-fluorene-2-amine

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 85 ℃; for 12h; Inert atmosphere;

Reference yield: 79.0%

: 1347758-80-8
(N-[1,1‘-biphenyl]-4-yl)-9,9-dimethyl-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)phenyl)-9H-fluorene-2-amine

Guidance literature:: With (bis(tricyclohexyl)phosphine)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; for 12h; Reflux;

Reference yield: 70.0%

: 897671-69-1
N?(biphenyl?4?yl)?9,9?dimethyl?9H?fluorene?2?amine

: 68716-49-4
p-bromophenylboronic acid pinacol ester

: 1347758-80-8
(N-[1,1‘-biphenyl]-4-yl)-9,9-dimethyl-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)phenyl)-9H-fluorene-2-amine

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate; In toluene; at 100 ℃; for 7h; Inert atmosphere;