BENZYLOXY-3-CHLORO-2-PROPANOL

Base Information

• Chemical Name: BENZYLOXY-3-CHLORO-2-PROPANOL
• CAS No.: 103024-85-7
• Molecular Formula: C₁₀H₁₃ClO₂
• Molecular Weight: 200.665
• Mol file: 103024-85-7.mol

Synonyms:BENZYLOXY-3-CHLORO-2-PROPANOL

Chemical Property of BENZYLOXY-3-CHLORO-2-PROPANOL

Chemical Property:

• PSA: 29.46000
• LogP: 2.14890

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BENZYLOXY-3-CHLORO-2-PROPANOL

There total 35 articles about BENZYLOXY-3-CHLORO-2-PROPANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

epichlorohydrin (106-89-8,24969-06-0,13403-37-7) + benzyl alcohol (100-51-6,185532-71-2) → (R)-1-(benzyloxy)-3-chloropropan-2-ol (103024-85-7)

Guidance literature:

In acetonitrile; at 4 ℃; for 20h; enantioselective reaction;

DOI:10.1016/j.tet.2014.03.043

Reference yield: 96.0%

Benzyloxymethyl-oxiran (2930-05-4) → 1-chloro-2-hydroxy-3-phenylmethoxypropane (13991-52-1,103024-85-7)

Guidance literature:

With lithium chloride; 1-hexyl-3-methylimidazolium perchlorate; at 60 ℃; for 2h;

DOI:10.1055/s-2006-941562

Reference yield: 86.0%

epichlorohydrin (106-89-8,24969-06-0,13403-37-7) + benzyl alcohol (100-51-6,185532-71-2) → 1-chloro-2-hydroxy-3-phenylmethoxypropane (13991-52-1,103024-85-7)

Guidance literature:

With organotin phosphate; In hexane; for 48h; Ambient temperature;

DOI:10.1016/S0040-4039(00)98156-5

upstream raw materials:

epichlorohydrin

benzyl alcohol

iodomethylbenzene

3-monochloro-1,2-propanediol

Downstream raw materials:

4-(1-benzyloxy-3-chloroisopropoxy)azetidin-2-one

1-benzyloxy-3-(2-methoxy-phenoxy)-propan-2-ol

1-benzyloxy-2-carbamoyloxy-3-(2-methoxy-phenoxy)-propane

tert-butyl 4-[acetyl(tert-butoxycarbonyl)amino]-6-(benzyloxymethyl)-3-oxo-5H-1,2,4-triazine-2-carboxylate

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