4-bromo-2-(trifluoromethoxy)benzenemethan amine

Base Information

• Chemical Name: 4-bromo-2-(trifluoromethoxy)benzenemethan amine
• CAS No.: 947583-96-2
• Molecular Formula: C8H7BrF3NO
• Molecular Weight: 270.049
• Mol file: 947583-96-2.mol

Synonyms:4-bromo-2-(trifluoromethoxy)benzenemethan amine

Chemical Property of 4-bromo-2-(trifluoromethoxy)benzenemethan amine

Chemical Property:

• PSA: 35.25000
• LogP: 3.50670

Purity/Quality:

99% ^*data from raw suppliers

(4-Bromo-2-(trifluoromethoxy)phenyl)methanamine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-bromo-2-(trifluoromethoxy)benzenemethan amine

There total 6 articles about 4-bromo-2-(trifluoromethoxy)benzenemethan amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-(4-bromo-2-(trifluoromethoxy)benzyl)isoindoline-1,3-dione → 1-{4-bromo-2-[(trifluoromethyl)oxy]phenyl}methanamine (947583-96-2)

Guidance literature:

With hydrazine hydrate; In methanol; at 60 ℃; for 2h;

Reference yield: 83.0%

4-bromo-2-[(trifluoromethyl)oxy]benzaldehyde (220996-80-5) → 1-{4-bromo-2-[(trifluoromethyl)oxy]phenyl}methanamine (947583-96-2)

Guidance literature:

With sodium tetrahydroborate; ammonia; In methanol; at 20 ℃; for 16h;

DOI:10.1016/j.bmcl.2009.08.074

Reference yield:

C8H5BrF3NO → 1-{4-bromo-2-[(trifluoromethyl)oxy]phenyl}methanamine (947583-96-2)

Guidance literature:

C₈H₅BrF₃NO; With sodium tetrahydroborate; In methanol; at 20 ℃; for 3h;

With hydrogenchloride; In water;

upstream raw materials:

4-bromo-2-[(trifluoromethyl)oxy]benzaldehyde

(4-bromo-2-(trifluoromethoxy)phenyl)methanol

4-bromo-2-(trifluoromethoxy)benzyl methanesulfonate

Downstream raw materials:

1-benzyl-N-(4-bromo-2-(trifluoromethoxy)benzyl)-2,6-dioxo-1,2,3,6-tetrahydropyrimidine-4-carboxamide

N-(4-bromo-2-(trifluoromethoxy)benzyl)piperidine-4-carboxamide

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