3-ethylpentyl broMide

Base Information

• Chemical Name: 3-ethylpentyl broMide
• CAS No.: 1647-24-1
• Molecular Formula: C7H15Br
• Molecular Weight: 179.098
• Mol file: 1647-24-1.mol

Synonyms:3-ethylpentyl broMide

Chemical Property of 3-ethylpentyl broMide

Chemical Property:

• PSA: 0.00000
• LogP: 3.20760

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-ethylpentyl broMide

There total 1 articles about 3-ethylpentyl broMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-ethyl-1-pentene (4038-04-4) → 3-ethylpentyl bromide (1647-24-1)

Guidance literature:

Multistep reaction; (i) 9-BBN, THF, (ii) Br₂, CH₂Cl₂;

Reference yield: 88.0%

3-ethylpentyl bromide (1647-24-1) + N-methyl-N-phenyl-2-(2-aminophenoxy)acetamide (184870-82-4) → N-methyl-N-phenyl-2-<2-phenoxy>acetamide (237747-89-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 48h;

DOI:10.1248/cpb.47.755

Reference yield:

3-ethylpentyl bromide (1647-24-1) → N-methyl-N-phenyl-2-<2-phenoxy>acetamide (237748-11-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 88 percent / K₂CO₃ / dimethylformamide / 48 h / 70 °C

2: pyridine / CH₂Cl₂ / 1 h / Ambient temperature

3: hydrazine monohydrate / ethanol; CHCl₃ / Ambient temperature

With pyridine; potassium carbonate; hydrazine hydrate; In ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide;

DOI:10.1248/cpb.47.755

upstream raw materials:

3-ethyl-1-pentene

Downstream raw materials:

N-methyl-N-phenyl-2-<2-phenoxy>acetamide

N-methyl-N-phenyl-2-<2-phenoxy>acetamide

(+/-)-N-methyl-N-phenyl-2-<2-amino>phenoxy>acetamide

methyl 2-<3-<3-carbamoylmethyl>ureido>phenyl>acetate