2-chloro-3-[[(2-propen-1-yloxy)carbonyl]amino]benzoic acid methyl ester

Base Information

Chemical Name:2-chloro-3-[[(2-propen-1-yloxy)carbonyl]amino]benzoic acid methyl ester
CAS No.:1195768-68-3
Molecular Formula:C₁₂H₁₂ClNO₄
Molecular Weight:269.685
Hs Code.:
Mol file:1195768-68-3.mol

Synonyms:2-chloro-3-[[(2-propen-1-yloxy)carbonyl]amino]benzoic acid methyl ester

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Chemical Property of 2-chloro-3-[[(2-propen-1-yloxy)carbonyl]amino]benzoic acid methyl ester

Chemical Property:

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Technology Process of 2-chloro-3-[[(2-propen-1-yloxy)carbonyl]amino]benzoic acid methyl ester

There total 3 articles about 2-chloro-3-[[(2-propen-1-yloxy)carbonyl]amino]benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120100-15-4
methyl 3-amino-2-chlorobenzoate

: 2937-50-0
Allyl chloroformate

: 1195768-68-3
methyl 2-chloro-3-{[(2-propen-1-yloxy)carbonyl]amino}benzoate

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: 53553-14-3
2-chloro-3-nitrobenzoic acid methyl ester

: 1195768-68-3
methyl 2-chloro-3-{[(2-propen-1-yloxy)carbonyl]amino}benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / methanol / 3.5 h / 25 °C / 2585.81 Torr / Inert atmosphere

2: sodium hydrogencarbonate / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

With hydrogen; sodium hydrogencarbonate; In tetrahydrofuran; methanol;

Reference yield:

: 3970-35-2
2-chloro-3-nitrobezoic acid

: 1195768-68-3
methyl 2-chloro-3-{[(2-propen-1-yloxy)carbonyl]amino}benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / Inert atmosphere; Reflux

2: hydrogen / methanol / 3.5 h / 25 °C / 2585.81 Torr / Inert atmosphere

3: sodium hydrogencarbonate / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

With hydrogen; sodium hydrogencarbonate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol;