3,4,6-Tri-O-acetyl-p-Nitrophenyl 2-Azido-2-deoxy-α-D-galactopyranoside

Base Information

Chemical Name:3,4,6-Tri-O-acetyl-p-Nitrophenyl 2-Azido-2-deoxy-α-D-galactopyranoside
CAS No.:1147438-51-4
Molecular Formula:C18H20N4O10
Molecular Weight:452.3722
Hs Code.:
Mol file:1147438-51-4.mol

Synonyms:3,4,6-Tri-O-acetyl-p-Nitrophenyl 2-Azido-2-deoxy-α-D-galactopyranoside;4-Nitrophenyl 2-Azido-2-deoxy-α-D-galactopyranoside 3,4,6-Triacetate

Suppliers and Price of 3,4,6-Tri-O-acetyl-p-Nitrophenyl 2-Azido-2-deoxy-α-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3,4,6-Tri-O-acetyl-p-Nitrophenyl2-Azido-2-deoxy-α-D-galactopyranoside
50 mg
$ 260.00

Medical Isotopes, Inc.
3-4-6-Tri-O-acetyl-p-nitrophenyl2-azido-2-deoxy-α-D-galactopyranoside
10 mg
$ 426.00

Biosynth Carbosynth
4-Nitrophenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-a-D-galactopyranoside
100 mg
$ 751.00

Biosynth Carbosynth
4-Nitrophenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-a-D-galactopyranoside
50 mg
$ 413.50

Biosynth Carbosynth
4-Nitrophenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-a-D-galactopyranoside
10 mg
$ 125.10

Total 2 raw suppliers

Chemical Property of 3,4,6-Tri-O-acetyl-p-Nitrophenyl 2-Azido-2-deoxy-α-D-galactopyranoside

Chemical Property:

PSA：192.93000
LogP:1.77986
Solubility.:Chloroform, Dichloromethane, Ethyl Acetate, Methanol

Purity/Quality:

97% ^*data from raw suppliers

3,4,6-Tri-O-acetyl-p-Nitrophenyl2-Azido-2-deoxy-α-D-galactopyranoside ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses 3,4,6-Tri-O-acetyl-p-Nitrophenyl 2-Azido-2-deoxy-α-D-galactopyranoside (cas# 1147438-51-4) is a compound useful in organic synthesis.

Technology Process of 3,4,6-Tri-O-acetyl-p-Nitrophenyl 2-Azido-2-deoxy-α-D-galactopyranoside

There total 1 articles about 3,4,6-Tri-O-acetyl-p-Nitrophenyl 2-Azido-2-deoxy-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 83025-20-1
3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyltrichloroacetimidate

: 1147438-51-4
p-nitrophenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 ℃;
DOI:10.1016/j.carres.2011.03.036

Reference yield:

: 1147438-51-4
p-nitrophenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranoside

: 210418-04-5
C₁₂H₁₄N₄O₇

Guidance literature:: p-nitrophenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranoside; With sodium methylate; In methanol; at 20 ℃; for 0.5h; pH=10;

In methanol;
DOI:10.1016/j.carres.2011.03.036

Reference yield:

: 1147438-51-4
p-nitrophenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranoside

: 1316823-00-3
p-nitrophenyl 2-azido-3-O-benzoyl-2-deoxy-4,6-O-p-methoxybenzylidene-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate / methanol / 0.5 h / 20 °C / pH 10

1.2: Dowex H+

2.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide; acetonitrile / 1 h / 20 °C

3.1: pyridine / 1 h / 0 °C / Cooling with ice

With sodium methylate; toluene-4-sulfonic acid; In pyridine; methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.carres.2011.03.036