ETHYL 2,6-DIMETHYLBENZOYLFORMATE

Base Information

• Chemical Name: ETHYL 2,6-DIMETHYLBENZOYLFORMATE
• CAS No.: 698392-47-1
• Molecular Formula: C12H14O3
• Molecular Weight: 206.24
• Hs Code.: 2918300090
• Mol file: 698392-47-1.mol

Synonyms:ETHYL 2,6-DIMETHYLBENZOYLFORMATE

Chemical Property of ETHYL 2,6-DIMETHYLBENZOYLFORMATE

Chemical Property:

• Vapor Pressure: 0.000406mmHg at 25°C
• Boiling Point: 316.6°C at 760 mmHg
• Flash Point: 141.4°C
• PSA: 43.37000
• Density: 1.085g/cm³
• LogP: 2.04920

Purity/Quality:

99% ^*data from raw suppliers

(2,6-Dimethylphenyl)oxoaceticacidethylester ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 22

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ETHYL 2,6-DIMETHYLBENZOYLFORMATE

There total 4 articles about ETHYL 2,6-DIMETHYLBENZOYLFORMATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2,6-dimethyl-1-chlorobenzene (6781-98-2) + Ethyl oxalyl chloride (4755-77-5) → ethyl (2,6-dimethylphenyl)-2-oxoacetate (698392-47-1)

Guidance literature:

2,6-dimethyl-1-chlorobenzene; With lithium; In diethyl ether; at 3 - 6 ℃;

With copper(l) cyanide; In tetrahydrofuran; diethyl ether; at -80 - -25 ℃; for 0.416667h;

Ethyl oxalyl chloride; In tetrahydrofuran; diethyl ether; at -80 ℃;

DOI:10.1021/ol302672n

Reference yield:

2,6-dimethylstyrene (2039-90-9) → ethyl (2,6-dimethylphenyl)-2-oxoacetate (698392-47-1)

Guidance literature:

With potassium hydroxide; potassium permanganate; Erwaermen des Reaktionsprodukts mit H₂SO₄, Aethanol und Benzol;

DOI:10.1021/ja01632a043

Reference yield:

2,6-dimethyliodobenzene (608-28-6) → ethyl (2,6-dimethylphenyl)-2-oxoacetate (698392-47-1)

Guidance literature:

Multi-step reaction with 3 steps

1: lithium; diethyl ether / anschliessend Behandeln mit Acetaldehyd

2: activated Al₂O₃ / 270 - 280 °C / 10 Torr

3: KMnO₄; aqueous KOH / Erwaermen des Reaktionsprodukts mit H₂SO₄, Aethanol und Benzol

With aluminum oxide; potassium hydroxide; potassium permanganate; diethyl ether; lithium;

DOI:10.1021/ja01632a043

upstream raw materials:

2,6-dimethylstyrene

2,6-dimethyliodobenzene

rac-1-(2,6-dimethylphenyl)ethan-1-ol

2,6-dimethyl-1-chlorobenzene

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