5-Amino-3-methyl-1-(3-nitrophenyl)-1H-pyrazole-4-carbonitrile

Base Information

• Chemical Name: 5-Amino-3-methyl-1-(3-nitrophenyl)-1H-pyrazole-4-carbonitrile
• CAS No.: 107842-58-0
• Molecular Formula: C₁₁H₉N₅O₂
• Molecular Weight: 243.225
• Hs Code.: 2933199090
• Mol file: 107842-58-0.mol

Synonyms:5-Amino-3-methyl-1-(3-nitrophenyl)-1H-pyrazole-4-carbonitrile;5-Amino-4-cyano-3-methyl-1-(3-nitrophenyl)pyrazole

Chemical Property of 5-Amino-3-methyl-1-(3-nitrophenyl)-1H-pyrazole-4-carbonitrile

Chemical Property:

• PSA: 113.45000
• LogP: 2.64718
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

5-Amino-4-cyano-3-methyl-1-(3-nitrophenyl)pyrazole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 5-Amino-4-cyano-3-methyl-1-(3-nitrophenyl)pyrazole is used as a reactant in the preparation of phenylpyrazole derivatives as novel anti-HIV agents.

Technology Process of 5-Amino-3-methyl-1-(3-nitrophenyl)-1H-pyrazole-4-carbonitrile

There total 2 articles about 5-Amino-3-methyl-1-(3-nitrophenyl)-1H-pyrazole-4-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-nitrophenylhydrazine (619-27-2) + (1-ethoxyethylidene)malononitrile (5417-82-3) → 5-amino-3-methyl-1-(3-nitrophenyl)-1H-pyrazole-4-carbonitrile (107842-58-0)

Guidance literature:

In ethanol; at 20 ℃;

DOI:10.1016/j.bmcl.2013.06.026

Reference yield:

→ 5-amino-3-methyl-1-(3-nitrophenyl)-1H-pyrazole-4-carbonitrile (107842-58-0)

Guidance literature:

With triethylamine; In ethanol; at 20 ℃; for 0.333333h;

In ethanol; at 20 ℃; for 1h;

Reference yield:

5-amino-3-methyl-1-(3-nitrophenyl)-1H-pyrazole-4-carbonitrile (107842-58-0) + N-(3-chloro-5-formyl-2-hydroxyphenyl)propionamide (1448812-08-5) → C21H17ClN6O4

Guidance literature:

With pyridinium p-toluenesulfonate; In toluene; Reflux;

DOI:10.1016/j.bmcl.2013.06.026

upstream raw materials:

3-nitrophenylhydrazine

(1-ethoxyethylidene)malononitrile

Downstream raw materials:

N-(3-chloro-5-(((4-cyano-3-methyl-1-(3-nitrophenyl)-1H-pyrazol-5-yl)amino)methyl)-2-hydroxyphenyl)propionamide

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