2-(HydroxyiMino)-3-oxo-pentanedioic Acid 1,5-Diethyl Ester

Base Information

• Chemical Name: 2-(HydroxyiMino)-3-oxo-pentanedioic Acid 1,5-Diethyl Ester
• CAS No.: 996-75-8
• Molecular Formula: C9H13NO6
• Molecular Weight: 231.205
• Mol file: 996-75-8.mol

Synonyms:2-(HydroxyiMino)-3-oxo-pentanedioic Acid 1,5-Diethyl Ester;2-(HydroxyiMino)-3-oxo-pentanedioic Acid Diethyl Ester;2,3-Dioxo-glutaric Acid Diethyl Ester 2-OxiMe

Chemical Property of 2-(HydroxyiMino)-3-oxo-pentanedioic Acid 1,5-Diethyl Ester

Chemical Property:

• PSA: 102.26000
• LogP: -0.09800
• Solubility.: Dichloromethane, Diethyl Ether, Ethyl Acetate

Purity/Quality:

99% ^*data from raw suppliers

2-(Hydroxyimino)-3-oxo-pentanedioicAcid1,5-DiethylEster ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2-(HydroxyiMino)-3-oxo-pentanedioic Acid 1,5-Diethyl Ester is used in the preparation of Isoxazole derivatives.

Technology Process of 2-(HydroxyiMino)-3-oxo-pentanedioic Acid 1,5-Diethyl Ester

There total 5 articles about 2-(HydroxyiMino)-3-oxo-pentanedioic Acid 1,5-Diethyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

diethyl 1,3-acetonedicarboxylate (105-50-0) → diethyl 2-nitroso-3-ketoglutarate (996-75-8)

Guidance literature:

With acetic acid; sodium nitrite; at 5 - 7 ℃; for 0.166667h;

Reference yield:

ethyl nitrite (109-95-5) + diethyl 1,3-acetonedicarboxylate (105-50-0) → diethyl 2-nitroso-3-ketoglutarate (996-75-8)

Guidance literature:

With hydrogenchloride;

Reference yield:

diethyl 1,3-acetonedicarboxylate (105-50-0) + isopentyl nitrite (110-46-3) → diethyl 2-nitroso-3-ketoglutarate (996-75-8)

Guidance literature:

With hydrogenchloride;

upstream raw materials:

ethyl nitrite

diethyl 1,3-acetonedicarboxylate

isopentyl nitrite

Downstream raw materials:

threo-β-hydroxyglutamic acid

erythro-3-hydroxyglutamic acid

2-amino-3-hydroxypentanedioic acid

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