3,4-dimethylbenzohydrazide

Base Information

• Chemical Name: 3,4-dimethylbenzohydrazide
• CAS No.: 42596-61-2
• Molecular Formula: C9H12N2O
• Molecular Weight: 164.2
• Hs Code.: 2928000090
• Mol file: 42596-61-2.mol

Synonyms:3,4-dimethylbenzohydrazide;3,4-DIMETHYL-BENZOIC ACID HYDRAZIDE;UKRORGSYN-BB BBV-041472;VITAS-BB TBB008446;3,4-dimethylbenzohydrazide(SALTDATA: FREE);3,5-Dimethylbenzoic acid hydrazide

Chemical Property of 3,4-dimethylbenzohydrazide

Chemical Property:

• PKA: 12.85±0.10(Predicted)
• PSA: 55.12000
• Density: 1.098g/cm³
• LogP: 1.99810

Purity/Quality:

97% ^*data from raw suppliers

3,4-dimethylbenzohydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,4-dimethylbenzohydrazide

There total 2 articles about 3,4-dimethylbenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

methyl 3,4-dimethylbenzoate (38404-42-1) → 3,4-dimethylbenzoylhydrazine (42596-61-2)

Guidance literature:

With hydrazine hydrate; at 100 ℃; for 6h;

DOI:10.1021/ma035576y

Reference yield:

→ 3,4-dimethylbenzoylhydrazine (42596-61-2)

Guidance literature:

entspr. Ethylester + Hydrazin;

Reference yield: 85.0%

3,4-dimethylbenzoylhydrazine (42596-61-2) + benzoyl chloride (98-88-4) → N-(3,4-dimethylbenzoyl)-N'-benzoylhydrazine (775302-11-9)

Guidance literature:

With pyridine; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 4h;

DOI:10.1021/ma035576y

upstream raw materials:

methyl 3,4-dimethylbenzoate

Downstream raw materials:

N-(3,4-dimethylbenzoyl)-N'-benzoylhydrazine

[2-(diethoxy-phosphorylmethyl)-5-(5-phenyl-[1,3,4]oxadiazol-2-yl)-benzyl]-phosphonic acid diethyl ester