Pyridin-2-ylmethanesulfonamide

Base Information

• Chemical Name: Pyridin-2-ylmethanesulfonamide
• CAS No.: 889954-95-4
• Molecular Formula: C6H8N2O2S
• Molecular Weight: 172.208
• European Community (EC) Number: 858-914-8

Synonyms:pyridin-2-ylmethanesulfonamide;889954-95-4;1-Pyridin-2-ylmethanesulfonamide;PYRIDIN-2-YL-METHANESULFONAMIDE;pyridylmethylsulfonamide;SCHEMBL51377;(pyridin-2-yl)methanesulfonamide;YNRCVVBNEPJYOF-UHFFFAOYSA-N;SB13089;AM101501;DB-329015;CS-0105942;EN300-69257;D76578;Z385450902

Chemical Property of Pyridin-2-ylmethanesulfonamide

Chemical Property:

• PSA: 81.43000
• LogP: 1.65120
• XLogP3: -0.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 172.03064868
• Heavy Atom Count: 11
• Complexity: 207

Purity/Quality:

97% ^*data from raw suppliers

pyridin-2-ylmethanesulfonamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=NC(=C1)CS(=O)(=O)N

Technology Process of Pyridin-2-ylmethanesulfonamide

There total 2 articles about Pyridin-2-ylmethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(methoxymethyl)pyridine (23579-92-2) + O-(methylsulfonyl)hydroxylamine (61017-18-3) → pyridin-2-ylmethanesulfonamide (889954-95-4)

Guidance literature:

With sodium acetate; In water; at 20 ℃; for 48h;

Reference yield:

→ pyridin-2-ylmethanesulfonamide (889954-95-4)

Guidance literature:

With potassium carbonate; In methanol; at 20 ℃; for 0.166667h;

With hydroxylamine-O-sulfonic acid; In methanol; water; at 20 ℃;

Reference yield: 37.0%

pyridin-2-ylmethanesulfonamide (889954-95-4) + 8-cyclohexyl-11-methoxy-1a-((3-methyl-3,8-diazabicyclo[3.2.1]oct-8-yl)carbonyl)-1,1a,2,12b-tetrahydrocyclopropa[d]indolo[2,1-a][2]benzazepine-5-carboxylic acid trifluoroacetate → 8-cyclohexyl-11-methoxy-1a-((3-methyl-3,8-diazabicyclo[3.2.1]oct-8-yl)carbonyl)-N-((2-pyridinylmethyl)sulfonyl)-1,1a,2,12b-tetrahydrocyclopropa[d]indolo[2,1-a][2]benzazepine-5-carboxamide

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; sealed vial;

upstream raw materials:

2-(methoxymethyl)pyridine

O-(methylsulfonyl)hydroxylamine

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