1,3-Benzodioxole, 5-(phenylmethoxy)-

Base Information

Chemical Name:1,3-Benzodioxole, 5-(phenylmethoxy)-
CAS No.:66177-24-0
Molecular Formula:C14H12O3
Molecular Weight:228.247
Hs Code.:
DSSTox Substance ID:DTXSID60216362
Nikkaji Number:J1.477.708C
Wikidata:Q83092584
Pharos Ligand ID:S5DT5WJUNDMY
ChEMBL ID:CHEMBL144555

Synonyms:1,3-Benzodioxole, 5-(phenylmethoxy)-;AI3-21086;CHEMBL144555;66177-24-0;5-phenylmethoxy-1,3-benzodioxole;SCHEMBL4731619;5-Benzyloxy-benzo[1,3]dioxole;DTXSID60216362;5-(Benzyloxy)-1,3-benzodioxole;JEUUXPKQEVMAEC-UHFFFAOYSA-N;BDBM50409085;5-(Benzyloxy)benzo[d][1,3]dioxole;AKOS008408642;SY309778

Suppliers and Price of 1,3-Benzodioxole, 5-(phenylmethoxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1,3-Benzodioxole, 5-(phenylmethoxy)-

Chemical Property:

Vapor Pressure:0.00013mmHg at 25°C
Boiling Point:344.6°Cat760mmHg
Flash Point:115.9°C
Density:1.231g/cm³
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:228.078644241
Heavy Atom Count:17
Complexity:238

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1OC2=C(O1)C=C(C=C2)OCC3=CC=CC=C3

Technology Process of 1,3-Benzodioxole, 5-(phenylmethoxy)-

There total 5 articles about 1,3-Benzodioxole, 5-(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 533-31-3
Sesamol

: 100-39-0
benzyl bromide

: 66177-24-0
5-(benzyloxy)benzo[d][1,3]dioxole

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 23 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1021/jo400670y

Reference yield: 93.0%

: 533-31-3
Sesamol

: 100-44-7
benzyl chloride

: 66177-24-0
5-(benzyloxy)benzo[d][1,3]dioxole

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1080/10286020.2011.653561

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 66177-24-0
5-(benzyloxy)benzo[d][1,3]dioxole

Guidance literature:: Multi-step reaction with 2 steps

1.1: H₂O₂; formic acid / CH₂Cl₂; H₂O / 18 h / Heating

1.2: 77 percent / NaOH / CH₂Cl₂; H₂O / 0.25 h / 20 °C

2.1: 95 percent / potassium carbonate / dimethylformamide / 20 h / 20 °C

With formic acid; dihydrogen peroxide; potassium carbonate; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.07.046