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4,4,5,5-tetraMethyl-2-(perylen-3-yl)-1,3,2-dioxaborolane

Base Information Edit
  • Chemical Name:4,4,5,5-tetraMethyl-2-(perylen-3-yl)-1,3,2-dioxaborolane
  • CAS No.:950761-81-6
  • Molecular Formula:C26H23BO2
  • Molecular Weight:378.278
  • Hs Code.:2934999090
  • Mol file:950761-81-6.mol
4,4,5,5-tetraMethyl-2-(perylen-3-yl)-1,3,2-dioxaborolane

Synonyms:4,4,5,5-tetraMethyl-2-(perylen-3-yl)-1,3,2-dioxaborolane;4,4,5,5-Tetramethyl-2-(3-perylenyl)-1,3,2-dioxaborolane;(3-Perylenyl)boronic acid pinacol ester

Suppliers and Price of 4,4,5,5-tetraMethyl-2-(perylen-3-yl)-1,3,2-dioxaborolane
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
  • TCI Chemical
  • 4,4,5,5-Tetramethyl-2-(3-perylenyl)-1,3,2-dioxaborolane >97.0%(GC)
  • 200mg
  • $ 176.00
  • TCI Chemical
  • 4,4,5,5-Tetramethyl-2-(3-perylenyl)-1,3,2-dioxaborolane >97.0%(GC)
  • 1g
  • $ 615.00
  • Matrix Scientific
  • 4,4,5,5-Tetramethyl-2-(perylen-3-yl)-1,3,2-dioxaborolane 97%
  • 10g
  • $ 3240.00
  • Matrix Scientific
  • 4,4,5,5-Tetramethyl-2-(perylen-3-yl)-1,3,2-dioxaborolane 97%
  • 5g
  • $ 2160.00
  • Alichem
  • 4,4,5,5-Tetramethyl-2-(perylen-3-yl)-1,3,2-dioxaborolane
  • 1g
  • $ 480.76
  • AK Scientific
  • 4,4,5,5-Tetramethyl-2-(perylen-3-yl)-1,3,2-dioxaborolane
  • 10g
  • $ 4424.00
Total 14 raw suppliers
Chemical Property of 4,4,5,5-tetraMethyl-2-(perylen-3-yl)-1,3,2-dioxaborolane Edit
Chemical Property:
  • Melting Point:234.0 to 238.0 °C 
  • Boiling Point:570.4±19.0 °C(Predicted) 
  • PSA:18.46000 
  • Density:1.21±0.1 g/cm3(Predicted) 
  • LogP:6.03640 
  • Solubility.:slightly sol. in Chloroform 
Purity/Quality:

97% *data from raw suppliers

4,4,5,5-Tetramethyl-2-(3-perylenyl)-1,3,2-dioxaborolane >97.0%(GC) *data from reagent suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
Technology Process of 4,4,5,5-tetraMethyl-2-(perylen-3-yl)-1,3,2-dioxaborolane

There total 7 articles about 4,4,5,5-tetraMethyl-2-(perylen-3-yl)-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; at 70 ℃; for 15h;
DOI:10.1021/jo702019p
Guidance literature:
3-bromoperylene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Schlenk technique; Inert atmosphere;
Triisopropyl borate; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h; Schlenk technique; Inert atmosphere;
2,3-dimethyl-2,3-butane diol; In tetrahydrofuran; hexane; at 20 ℃; for 69h; Schlenk technique; Inert atmosphere;
DOI:10.1002/chem.202102052
Guidance literature:
PERYLENE; bis(pinacol)diborane; With bis(1,5-cyclooctadiene)nickel(0); 1,2-bis-(dicyclohexylphosphino)ethane; In 5,5-dimethyl-1,3-cyclohexadiene; at 20 ℃; for 0.166667h; Schlenk technique; Inert atmosphere; Sealed tube;
With 2,2,2-trifluoroethanol; In 5,5-dimethyl-1,3-cyclohexadiene; at 80 ℃; for 36h; regioselective reaction; Schlenk technique; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.joc.9b02333
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