2-Bicyclo(2.2.1)hept-2-ylideneethanamine

Base Information

• Chemical Name: 2-Bicyclo(2.2.1)hept-2-ylideneethanamine
• CAS No.: 80106-52-1
• Molecular Formula: C₉H₁₅N
• Molecular Weight: 137.225
• DSSTox Substance ID: DTXSID401232668
• Mol file: 80106-52-1.mol

Synonyms:2-(bicyclo(2.2.1)hept-2-ylidene)ethanamine;2-BCHYE-ET

Chemical Property of 2-Bicyclo(2.2.1)hept-2-ylideneethanamine

Chemical Property:

• Vapor Pressure: 0.0569mmHg at 25°C
• Boiling Point: 233.1°C at 760 mmHg
• Flash Point: 102.9°C
• Density: 1.088g/cm³
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 137.120449483
• Heavy Atom Count: 10
• Complexity: 160

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1CC2CC1CC2=CCN
• Isomeric SMILES: C1CC\2CC1C/C2=C\CN

Technology Process of 2-Bicyclo(2.2.1)hept-2-ylideneethanamine

There total 2 articles about 2-Bicyclo(2.2.1)hept-2-ylideneethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

(bicyclo<2.2.1>hept-2-ylidene)acetonitrile → 2-(bicyclo<2.2.1>hept-2-ylidene)ethanamine (80106-52-1)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; 1.) reflux, 2 h; 2.) 12 h, r.t.;

Reference yield:

2-norbornanone (497-38-1,2630-41-3,22270-13-9,29583-35-5) → 2-(bicyclo<2.2.1>hept-2-ylidene)ethanamine (80106-52-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / 85percent KOH / 24 h / Heating

2: 73 percent / LiAlH₄ / diethyl ether / 1.) reflux, 2 h; 2.) 12 h, r.t.

With potassium hydroxide; lithium aluminium tetrahydride; In diethyl ether;

upstream raw materials:

2-norbornanone

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