11-Dicyclohexylphosphino-12-phenyl-9,10-ethenoanthracene dichloromethane adduct, min. 98% KITPHOS

Base Information

Chemical Name:11-Dicyclohexylphosphino-12-phenyl-9,10-ethenoanthracene dichloromethane adduct, min. 98% KITPHOS
CAS No.:1166994-77-9
Molecular Formula:C34H37P
Molecular Weight:476.642
Hs Code.:
Mol file:1166994-77-9.mol

Synonyms:11-Dicyclohexylphosphino-12-phenyl-9,10-ethenoanthracene dichloromethane adduct, min. 98% KITPHOS;Dicyclohexyl(9,10-dihydro-12-phenyl-9,10-ethenoanthracen-11-yl)phosphine;11-Dicyclohexylphosphino-12-phenyl-9,10-ethenoanthracene dichloromethane adduct

Suppliers and Price of 11-Dicyclohexylphosphino-12-phenyl-9,10-ethenoanthracene dichloromethane adduct, min. 98% KITPHOS

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Strem Chemicals
11-Dicyclohexylphosphino-12-phenyl-9,10-ethenoanthracene dichloromethane adduct, min. 98% KITPHOS
500mg
$ 256.00

Strem Chemicals
11-Dicyclohexylphosphino-12-phenyl-9,10-ethenoanthracene dichloromethane adduct, min. 98% KITPHOS
100mg
$ 64.00

Total 6 raw suppliers

Chemical Property of 11-Dicyclohexylphosphino-12-phenyl-9,10-ethenoanthracene dichloromethane adduct, min. 98% KITPHOS

Chemical Property:

PSA：13.59000
LogP:9.83600

Purity/Quality:

97% ^*data from raw suppliers

11-Dicyclohexylphosphino-12-phenyl-9,10-ethenoanthracene dichloromethane adduct, min. 98% KITPHOS ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 11-Dicyclohexylphosphino-12-phenyl-9,10-ethenoanthracene dichloromethane adduct, min. 98% KITPHOS

There total 3 articles about 11-Dicyclohexylphosphino-12-phenyl-9,10-ethenoanthracene dichloromethane adduct, min. 98% KITPHOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1166994-74-6
11-(dicyclohexylphosphinoyl)-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

: 1166994-77-9
11-(dicyclohexylphosphino)-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

Guidance literature:: With trichlorosilane; triethylamine; In toluene; at 110 ℃; for 72h;
DOI:10.1002/adsc.200800307

Reference yield:

: 120-12-7
anthracene

: 1166994-77-9
11-(dicyclohexylphosphino)-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: neat (no solvent) / 12 - 22 h / 205 °C / Sealed tube

2: triethylamine; trichlorosilane / toluene / 40 h / 100 °C / Schlenk technique; Inert atmosphere

With trichlorosilane; triethylamine; In toluene; 1: |Diels-Alder Cycloaddition;
DOI:10.1021/om3011992

Reference yield:

: 1166994-71-3
dicyclohexyl(phenylethynyl)phosphine oxide

: 1166994-77-9
11-(dicyclohexylphosphino)-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: neat (no solvent) / 12 - 22 h / 205 °C / Sealed tube

2: triethylamine; trichlorosilane / toluene / 40 h / 100 °C / Schlenk technique; Inert atmosphere

With trichlorosilane; triethylamine; In toluene; 1: |Diels-Alder Cycloaddition;
DOI:10.1021/om3011992