11-(dicyclohexylphosphinoyl)-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

Base Information

Chemical Name:11-(dicyclohexylphosphinoyl)-12-phenyl-9,10-dihydro-9,10-ethenoanthracene
CAS No.:1166994-74-6
Molecular Formula:C₃₄H₃₇OP
Molecular Weight:492.641
Hs Code.:

Synonyms:11-(dicyclohexylphosphinoyl)-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 11-(dicyclohexylphosphinoyl)-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

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Technology Process of 11-(dicyclohexylphosphinoyl)-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

There total 1 articles about 11-(dicyclohexylphosphinoyl)-12-phenyl-9,10-dihydro-9,10-ethenoanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 120-12-7
anthracene

: 1166994-71-3
dicyclohexyl(phenylethynyl)phosphine oxide

: 1166994-74-6
11-(dicyclohexylphosphinoyl)-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

Guidance literature:: at 200 - 220 ℃;
DOI:10.1002/adsc.200800307

Reference yield: 69.0%

: 1166994-74-6
11-(dicyclohexylphosphinoyl)-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

: 1166994-77-9
11-(dicyclohexylphosphino)-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

Guidance literature:: With trichlorosilane; triethylamine; In toluene; at 110 ℃; for 72h;
DOI:10.1002/adsc.200800307

Reference yield:

: 1166994-74-6
11-(dicyclohexylphosphinoyl)-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

: 1415261-61-8
[Pd{κ²N2′,C1-2-(2′-NH₂C₆H₄)C₆H₄}Cl{11-(dicyclohexylphosphino)-12-phenyl-9,10-dihydro-9,10-ethenoanthracene}]

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; trichlorosilane / toluene / 40 h / 100 °C / Schlenk technique; Inert atmosphere

2: dichloromethane; acetone / 2 h / 20 °C

With trichlorosilane; triethylamine; In dichloromethane; acetone; toluene;
DOI:10.1021/om3011992