Bicyclo[2.2.1]hept-5-ene-2-carboxamide, 3-amino-, (1R,2S,3R,4S)-rel- (9CI)

Base Information

• Chemical Name: Bicyclo[2.2.1]hept-5-ene-2-carboxamide, 3-amino-, (1R,2S,3R,4S)-rel- (9CI)
• CAS No.: 105786-38-7
• Molecular Formula: C8H12N2O
• Molecular Weight: 152.19368
• Mol file: 105786-38-7.mol

Synonyms:Bicyclo[2.2.1]hept-5-ene-2-carboxamide, 3-amino-, (1R,2S,3R,4S)-rel- (9CI);3-endo-Aminobicyclo[2.2.1]hept-5-ene-2-endo-carboxamide,99+%

Chemical Property of Bicyclo[2.2.1]hept-5-ene-2-carboxamide, 3-amino-, (1R,2S,3R,4S)-rel- (9CI)

Chemical Property:

• PSA: 69.11000
• LogP: 1.02170

Purity/Quality:

(1R,2S,3R, 4S)-REL-3-AMINO-BICYCLO[2.2.1]HEPT-5-ENE-2-CARBOXAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bicyclo[2.2.1]hept-5-ene-2-carboxamide, 3-amino-, (1R,2S,3R,4S)-rel- (9CI)

There total 1 articles about Bicyclo[2.2.1]hept-5-ene-2-carboxamide, 3-amino-, (1R,2S,3R,4S)-rel- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

ethyl endo-3-aminobicyclo<2.2.1>hept-5-ene-2-endo-carboxylate (105786-34-3) → endo-3-aminobicyclo<2.2.1>hept-5-ene-endo-2-carboxamide (105786-38-7,402846-45-1)

Guidance literature:

With ammonia; In methanol; for 336h;

Reference yield: 92.0%

1-phenylmethyl-4-piperidone (3612-20-2) + endo-3-aminobicyclo<2.2.1>hept-5-ene-endo-2-carboxamide (105786-38-7,402846-45-1) → (4aS*,5R*,8S*,8aR*)-1′-benzyl-4a,5,8,8a-tetrahydro-1H-spiro[5,8-methanoquinazoline-2,4′-piperidin]-4(3H)-one

Guidance literature:

In ethanol; at 100 ℃; for 6h; under 7500.75 Torr; Solvent; Temperature; Flow reactor;

DOI:10.1002/ejoc.201800682

Reference yield: 48.0%

2-(4-toluoyl)benzoic acid (85-55-2) + endo-3-aminobicyclo<2.2.1>hept-5-ene-endo-2-carboxamide (105786-38-7,402846-45-1) → (1SR,4RS,4aSR,6aSR,12aRS)-6a-(p-tolyl)-1,4,4a,6,6a,12a-hexahydro-1,4-methanoisoindolo[2,1-a]quinazoline-5,11-dione

Guidance literature:

With toluene-4-sulfonic acid; In chlorobenzene; for 3h; Heating;

DOI:10.1016/j.molstruc.2004.02.039

upstream raw materials:

ethyl endo-3-aminobicyclo<2.2.1>hept-5-ene-2-endo-carboxylate

Downstream raw materials:

2-(4-chlorophenyl)-2,3,4ar,5t,8t,8ac-hexahydro-5,8-methano-4(1H)-quinazolinone

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