2-methyl-2,7-diazaspiro[4.5]decane(SALTDATA: FREE)

Base Information

Chemical Name:2-methyl-2,7-diazaspiro[4.5]decane(SALTDATA: FREE)
CAS No.:1086395-66-5
Molecular Formula:C9H18N2
Molecular Weight:154.255
Hs Code.:2933990090
Mol file:1086395-66-5.mol

Synonyms:2-methyl-2,7-diazaspiro[4.5]decane(SALTDATA: FREE);2,7-Diazaspiro[4.5]decane, 2-Methyl-;2-Methyl-2,7-diazaspiro[4.5]decane

Suppliers and Price of 2-methyl-2,7-diazaspiro[4.5]decane(SALTDATA: FREE)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Methyl-2,7-diazaspiro[4.5]decane
25mg
$ 45.00

Crysdot
2-Methyl-2,7-diazaspiro[4.5]decane 95+%
1g
$ 709.00

Chemenu
2-Methyl-2,7-diazaspiro[4.5]decane 95%
1g
$ 669.00

American Custom Chemicals Corporation
2-METHYL-2,7-DIAZASPIRO-[4.5]-DECANE 95.00%
5MG
$ 503.17

Total 7 raw suppliers

Chemical Property of 2-methyl-2,7-diazaspiro[4.5]decane(SALTDATA: FREE)

Chemical Property:

Boiling Point:200.3±8.0 °C(Predicted)
PKA:11.37±0.20(Predicted)
PSA：15.27000
Density:0.99±0.1 g/cm3(Predicted)
LogP:0.95840

Purity/Quality:

98%min ^*data from raw suppliers

2-Methyl-2,7-diazaspiro[4.5]decane ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-methyl-2,7-diazaspiro[4.5]decane(SALTDATA: FREE)

There total 17 articles about 2-methyl-2,7-diazaspiro[4.5]decane(SALTDATA: FREE) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1433194-47-8
2-methyl-2,7-diazaspiro[4.5]decane-1,3,8-trione

: 1086395-66-5
2-methyl-2,7-diazaspiro[4.5]decane

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2013.03.064

Reference yield: 60.0%

: 1153767-88-4
2-methyl-2,7-diazaspiro[4.5]decan-1-one hydrochloride

: 1086395-66-5
2-methyl-2,7-diazaspiro[4.5]decane

Guidance literature:: 2-methyl-2,7-diazaspiro[4.5]decan-1-one hydrochloride; With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 - 60 ℃; for 2h;

With sodium hydroxide; In tetrahydrofuran; water;

Reference yield:

: 6283-71-2
Dimethyl 1-cyanoethane-1,2-dicarboxylate

: 1086395-66-5
2-methyl-2,7-diazaspiro[4.5]decane

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / water / 3 h / 0 - 20 °C

2: hydrogen; platinum(IV) oxide / ethanol / 72 h / 5700.38 Torr / Autoclave

3: water / 20 - 170 °C

4: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux

With platinum(IV) oxide; lithium aluminium tetrahydride; hydrogen; triethylamine; In tetrahydrofuran; ethanol; water; 1: |Michael Addition;
DOI:10.1016/j.tet.2013.03.064