AKOS B018240

Base Information

• Chemical Name: AKOS B018240
• CAS No.: 359596-38-6
• Molecular Formula: C₁₂H₁₀N₂O₃S₂
• Molecular Weight: 294.355
• Hs Code.: 2934100090
• Mol file: 359596-38-6.mol

Synonyms:CHEMBRDG-BB 3018240;ART-CHEM-BB B018240;AKOS B018240;2-{4-[(E)-(2-mercapto-4-oxo-1,3-thiazol-5(4H)-ylidene)methyl]phenoxy}acetamide;Albb-009158;2-{4-[(E)-(2-mercapto-4-oxo-1,3-thiazol-5(4H)-ylidene)methyl]phenoxy}acetamide(SALTDATA: FREE);2-[4-[(E)-(4-keto-2-thioxo-thiazolidin-5-ylidene)methyl]phenoxy]acetamide;2-[4-[(E)-(4-oxo-2-sulfanylidene-1,3-thiazolidin-5-ylidene)methyl]phenoxy]acetamide

Chemical Property of AKOS B018240

Chemical Property:

• Vapor Pressure: 4.43E-13mmHg at 25°C
• Boiling Point: 571.7°C at 760 mmHg
• Flash Point: 299.6°C
• PSA: 145.85000
• Density: 1.521g/cm³
• LogP: 1.58670
• Storage Temp.: 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

2-{4-[(E)-(2-Mercapto-4-oxo-1,3-thiazol-5(4H)-ylidene)methyl]phenoxy}acetamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of AKOS B018240

There total 2 articles about AKOS B018240 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2-thioxo-4-thiazolidinone (141-84-4) + 2-(4-formyl-phenoxy)-acetamide (135857-20-4) → 2-[4-(4-oxo-2-thioxothiazolidin-5-ylidenemethyl)phenoxy]acetamide (359596-38-6)

Guidance literature:

With sodium acetate; acetic acid; Reflux;

DOI:10.1016/j.ejmech.2014.05.003

Reference yield:

4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → 2-[4-(4-oxo-2-thioxothiazolidin-5-ylidenemethyl)phenoxy]acetamide (359596-38-6)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / Reflux

2: sodium acetate; acetic acid / Reflux

With sodium acetate; potassium carbonate; acetic acid; In acetonitrile;

DOI:10.1016/j.ejmech.2014.05.003

upstream raw materials:

4-hydroxy-benzaldehyde

2-thioxo-4-thiazolidinone

2-(4-formyl-phenoxy)-acetamide

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