8-Methoxychroman-3-ol

Base Information

Chemical Name:8-Methoxychroman-3-ol
CAS No.:91520-01-3
Molecular Formula:C₁₀H₁₂O₃
Molecular Weight:180.203
Hs Code.:2932999099
DSSTox Substance ID:DTXSID10436412
Nikkaji Number:J243.063K
Mol file:91520-01-3.mol

Synonyms:8-methoxychroman-3-ol;91520-01-3;8-methoxy-3,4-dihydro-2H-chromen-3-ol;8-Methoxy-3-chromanol;DTXSID10436412;AKOS006311462;FT-0747114;8-METHOXY-3,4-DIHYDRO-2H-1-BENZOPYRAN-3-OL

Suppliers and Price of 8-Methoxychroman-3-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
8-Methoxychroman-3-ol
1g
$ 793.80

American Custom Chemicals Corporation
2,3-DIHYDRO-3-HYDROXY-8-METHOXY-(4H)-1-BENZOPYRAN 95.00%
5MG
$ 502.41

Chemenu
8-methoxychroman-3-ol 95%
1g
$ 757.00

Crysdot
8-Methoxychroman-3-ol 95+%
1g
$ 802.00

Total 13 raw suppliers

Chemical Property of 8-Methoxychroman-3-ol

Chemical Property:

Melting Point:80-82℃
PSA：38.69000
Density:1.215
LogP:0.99100
Storage Temp.:2-8°C
XLogP3:1.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:180.078644241
Heavy Atom Count:13
Complexity:172

Purity/Quality:

99%, ^*data from raw suppliers

8-Methoxychroman-3-ol ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC2=C1OCC(C2)O

Technology Process of 8-Methoxychroman-3-ol

There total 8 articles about 8-Methoxychroman-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 91520-04-6
8-methoxy-3,4-dihydro-2H-1-benzopyran-3-yl acetate

: 91520-01-3
3,4-dihydro-3-hydroxy-8-methoxy-2H-1-benzopyran

Guidance literature:: With sodium hydroxide; In methanol; for 1h; Ambient temperature;
DOI:10.1248/cpb.38.2088

Reference yield:

: 2173-78-6
2-Allyl-6-methoxyphenyl acetate

: 91520-01-3
3,4-dihydro-3-hydroxy-8-methoxy-2H-1-benzopyran

Guidance literature:: Multi-step reaction with 4 steps

1: 88.7 percent / 40 percent (w/v) peracetic acid, AcOK / CH₂Cl₂ / 48 h / Ambient temperature

2: 90.4 percent / 20 percent (w/v) HCl / diethyl ether / 12 h / Ambient temperature

3: 1.53 g / K₂CO₃ / dimethylformamide / 2 h / Ambient temperature

4: 52.1 percent / 1 N NaOH / methanol / 1 h / Ambient temperature

With hydrogenchloride; peracetic acid; sodium hydroxide; potassium acetate; potassium carbonate; In methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.35.632

Reference yield:

: 91520-02-4
2-(2,3-Epoxypropyl)-6-methoxyphenyl acetate

: 91520-01-3
3,4-dihydro-3-hydroxy-8-methoxy-2H-1-benzopyran

Guidance literature:: Multi-step reaction with 3 steps

1: 90.4 percent / 20 percent (w/v) HCl / diethyl ether / 12 h / Ambient temperature

2: 1.53 g / K₂CO₃ / dimethylformamide / 2 h / Ambient temperature

3: 52.1 percent / 1 N NaOH / methanol / 1 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; potassium carbonate; In methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1248/cpb.35.632