3-BROMO-4-IODOANILINE

Base Information

• Chemical Name: 3-BROMO-4-IODOANILINE
• CAS No.: 860435-38-7
• Molecular Formula: C6H5BrIN
• Molecular Weight: 297.921
• Hs Code.: 2921420090
• Mol file: 860435-38-7.mol

Synonyms:3-BROMO-4-IODOANILINE;3-Bromo-4-iodobenzenamine

Chemical Property of 3-BROMO-4-IODOANILINE

Chemical Property:

• Melting Point: 198 °C
• Boiling Point: 323.7±27.0 °C(Predicted)
• PKA: 2.73±0.10(Predicted)
• PSA: 26.02000
• Density: 2.292±0.06 g/cm3(Predicted)
• LogP: 3.21710
• Storage Temp.: Refrigerated.

Purity/Quality:

97% ^*data from raw suppliers

3-Bromo-4-iodoaniline 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-BROMO-4-IODOANILINE

There total 4 articles about 3-BROMO-4-IODOANILINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

m-Bromoaniline (591-19-5) → 3-bromo-4-iodoaniline (860435-38-7)

Guidance literature:

With N,N,N-trimethylbenzenemethanaminium dichloroiodate; calcium carbonate; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/ja042762q

Reference yield:

2-bromo-1-iodo-4-nitrobenzene (7149-14-6) → 3-bromo-4-iodoaniline (860435-38-7)

Guidance literature:

With iron; ammonium chloride; In ethanol; water; at 80 ℃; for 9h;

DOI:10.1002/chem.201605000

Reference yield:

2-bromo-4-nitroaniline (13296-94-1) → 3-bromo-4-iodoaniline (860435-38-7)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sulfuric acid; sodium nitrite / acetonitrile; water / 1 h / 0 °C

1.2: 1 h / 0 °C

2.1: iron; ammonium chloride / water; ethanol / 9 h / 80 °C

With sulfuric acid; iron; ammonium chloride; sodium nitrite; In ethanol; water; acetonitrile;

DOI:10.1002/chem.201605000

upstream raw materials:

m-Bromoaniline

2-bromo-4-nitroaniline

2-bromo-1-iodo-4-nitrobenzene

4-nitro-aniline

Downstream raw materials:

2-bromo-1,4-diiodobenzene

3-(bromo-4-iodophenyl)acetamide

1-(3-Bromo-4-iodo-phenyl)-3-(4-trifluoromethyl-phenyl)-urea

2,2'-dibromo-4-tert-butyl-[1,1';4',1'';4'',1''']quaterphenyl

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