BOC-L-ALANINE THIOAMIDE

Base Information

Chemical Name:BOC-L-ALANINE THIOAMIDE
CAS No.:96929-01-0
Molecular Formula:C₈H₁₆N₂O₂S
Molecular Weight:204.293
Hs Code.:2930909090
European Community (EC) Number:834-643-0
Nikkaji Number:J1.648.603E
Mol file:96929-01-0.mol

Synonyms:BOC-L-ALANINE THIOAMIDE;N-TERT-BUTOXYCARBONYL-L-THIOALANINAMIDE

Suppliers and Price of BOC-L-ALANINE THIOAMIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
tert-butylN-(1-carbamothioylethyl)carbamate
100mg
$ 285.00

American Custom Chemicals Corporation
BOC-L-ALANINE THIOAMIDE 95.00%
5MG
$ 495.69

AK Scientific
Tert-butylN-(1-carbamothioylethyl)carbamate
5g
$ 1288.00

AK Scientific
Tert-butylN-(1-carbamothioylethyl)carbamate
500mg
$ 418.00

Total 4 raw suppliers

Chemical Property of BOC-L-ALANINE THIOAMIDE

Chemical Property:

PSA：96.44000
Density:1.122±0.06 g/cm3(20 °C , 760mmHg)
LogP:2.27690
XLogP3:0.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:204.09324893
Heavy Atom Count:13
Complexity:211

Purity/Quality:

99% ^*data from raw suppliers

tert-butylN-(1-carbamothioylethyl)carbamate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C(=S)N)NC(=O)OC(C)(C)C

Technology Process of BOC-L-ALANINE THIOAMIDE

There total 12 articles about BOC-L-ALANINE THIOAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 78981-25-6,81587-17-9,85642-13-3
tert-butyl (1S)-2-amino-1-methyl-2-oxoethylcarbamate

: 141041-86-3,96929-01-0,140903-30-6
tert-butyl (S)-(1-amino-1-thioxopropan-2-yl)carbamate

Guidance literature:: With Lawessons reagent; In dichloromethane; at 20 ℃; for 16h;

Reference yield: 88.0%

: 141041-80-7
N-(tert-Butyloxycarbonyl)-DL-alaninnitril

: 96929-01-0
N-(tert-Butyloxycarbonyl)-DL-thioalaninamid

Guidance literature:: With pyridine; hydrogen sulfide; In tetrahydrofuran; at 0 ℃; for 7h;

Reference yield:

: 15761-38-3
L-N-Boc-Ala

: 141041-86-3,96929-01-0,140903-30-6
tert-butyl (S)-(1-amino-1-thioxopropan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 20 °C

1.2: 2 h / 20 °C

2.1: Lawessons reagent / dichloromethane / 12 h / 20 °C

With Lawessons reagent; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jo201675r