4-[3-(2-methoxyethyl)-4-methylpiperazin-1-yl]-2-(propan-2-yloxy)aniline

Base Information

Chemical Name:4-[3-(2-methoxyethyl)-4-methylpiperazin-1-yl]-2-(propan-2-yloxy)aniline
CAS No.:1462950-82-8
Molecular Formula:C₁₇H₂₉N₃O₂
Molecular Weight:307.436
Hs Code.:
Mol file:1462950-82-8.mol

Synonyms:4-[3-(2-methoxyethyl)-4-methylpiperazin-1-yl]-2-(propan-2-yloxy)aniline

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Chemical Property of 4-[3-(2-methoxyethyl)-4-methylpiperazin-1-yl]-2-(propan-2-yloxy)aniline

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Technology Process of 4-[3-(2-methoxyethyl)-4-methylpiperazin-1-yl]-2-(propan-2-yloxy)aniline

There total 6 articles about 4-[3-(2-methoxyethyl)-4-methylpiperazin-1-yl]-2-(propan-2-yloxy)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1462950-85-1
2-(2-methoxyethyl)-1-methyl-4-[4-nitro-3-(propan-2-yloxy)phenyl]piperazine

: 1462950-82-8
4-[3-(2-methoxyethyl)-4-methylpiperazin-1-yl]-2-(propan-2-yloxy)aniline

Guidance literature:: With palladium 10% on activated carbon; ammonium formate; In methanol; at 80 ℃; for 0.0833333h; Microwave irradiation;

Reference yield:

: 1462950-85-1
2-(2-methoxyethyl)-1-methyl-4-[4-nitro-3-(propan-2-yloxy)phenyl]piperazine

: 16712-16-6,64165-14-6,65387-22-6,70179-79-2,540-69-2
ammonium formate

: 1462950-82-8
4-[3-(2-methoxyethyl)-4-methylpiperazin-1-yl]-2-(propan-2-yloxy)aniline

Guidance literature:: With palladium 10% on activated carbon; In methanol; at 80 ℃; for 0.0833333h; Microwave irradiation;

Reference yield:

: 446-36-6
5-fluoro-2-nitrophenol

: 1462950-82-8
4-[3-(2-methoxyethyl)-4-methylpiperazin-1-yl]-2-(propan-2-yloxy)aniline

Guidance literature:: Multi-step reaction with 5 steps

1: caesium carbonate / N,N-dimethyl-formamide / 20 °C

2: N-ethyl-N,N-diisopropylamine / acetonitrile / 6 h / 110 °C

3: pyridine / dichloromethane / 20 °C

4: methanol / 0.67 h / 20 - 90 °C

5: palladium 10% on activated carbon / methanol / 0.08 h / 80 °C / Microwave irradiation

With pyridine; palladium 10% on activated carbon; caesium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;