HEXAKIS(2,3,6-TRI-O-METHYL)-ALPHA-CYCLODEXTRIN

Base Information

• Chemical Name: HEXAKIS(2,3,6-TRI-O-METHYL)-ALPHA-CYCLODEXTRIN
• CAS No.: 68715-56-0
• Molecular Formula: C54H96O30
• Molecular Weight: 1225.34
• Mol file: 68715-56-0.mol

Synonyms:HEXAKIS(2,3,6-TRI-O-METHYL)-ALPHA-CYCLODEXTRIN;ALPHA-CYCLODEXTRIN HEXAKIS(2,3,6-TRI-O-METHYL);Hexakis (2,3,6-tri-O-methyl)-α-cyclodextrin

Chemical Property of HEXAKIS(2,3,6-TRI-O-METHYL)-ALPHA-CYCLODEXTRIN

Chemical Property:

• PSA: 276.90000
• LogP: -1.28100
• Storage Temp.: 2-8°C
• Solubility.: Soluble in water, methanol, chloroform.

Purity/Quality:

99% ^*data from raw suppliers

Hexakis(2,3,6-tri-O-methyl)cylomaltohexaose ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of HEXAKIS(2,3,6-TRI-O-METHYL)-ALPHA-CYCLODEXTRIN

There total 8 articles about HEXAKIS(2,3,6-TRI-O-METHYL)-ALPHA-CYCLODEXTRIN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

alpha cyclodextrin (10016-20-3) + methyl iodide (74-88-4) → hexakis(2,3,6-tri-O-methyl)-α-cyclodextrin (68715-56-0)

Guidance literature:

alpha cyclodextrin; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 1.5h;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃;

DOI:10.1246/cl.2012.806

Reference yield:

alpha cyclodextrin (10016-20-3) + methyl iodide (74-88-4) → 2I-VI,6I-VI-dodeca-O-methylcyclomaltohexaose (51166-72-4) + hexakis(2,3,6-tri-O-methyl)-α-cyclodextrin (68715-56-0)

Guidance literature:

With sodium hydroxide; In dimethyl sulfoxide; Title compound not separated from byproducts;

Reference yield:

C56H98Cl3NO31 (848489-20-3) → hexakis(2,3,6-tri-O-methyl)-α-cyclodextrin (68715-56-0) + C54H96O30

Guidance literature:

With 4 A molecular sieve; boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃;

DOI:10.1039/b309261e

upstream raw materials:

dimethyl sulfate

alpha cyclodextrin

methyl iodide

C₅₆H₉₈Cl₃NO₃₁

Downstream raw materials:

C₆₀H₁₀₂O₃₀S

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