3aα,3bβ,6aβ,6bα-Tetrahydrocyclobuta[1,2-d:3,4-d']bis[1,3]dioxole

Base Information

• Chemical Name: 3aα,3bβ,6aβ,6bα-Tetrahydrocyclobuta[1,2-d:3,4-d']bis[1,3]dioxole
• CAS No.: 70004-63-6
• Molecular Weight: 144.13
• Mol file: 70004-63-6.mol

Synonyms:Cyclobuta[1,2-d:3,4-d']bis[1,3]dioxole, tetrahydro-, (3aα,3bβ,6aβ,6bα)- (9CI)

Chemical Property of 3aα,3bβ,6aβ,6bα-Tetrahydrocyclobuta[1,2-d:3,4-d']bis[1,3]dioxole

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3aα,3bβ,6aβ,6bα-Tetrahydrocyclobuta[1,2-d:3,4-d']bis[1,3]dioxole

There total 11 articles about 3aα,3bβ,6aβ,6bα-Tetrahydrocyclobuta[1,2-d:3,4-d']bis[1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-dioxole (288-53-9) → exo-bis-methylendioxy-cyclobutan (69956-59-8,70004-63-6,113428-72-1) + syn-dimeres-Dioxol (69956-59-8,70004-63-6,113428-72-1) + (1R,2R,6S,7S)-3,5-Dioxa-tricyclo[5.2.2.02,6]undec-8-ene + (1S,2R,6S,7R)-3,5-Dioxa-tricyclo[5.2.2.02,6]undec-8-ene

Guidance literature:

With 1,3-dioxole; tris-(4-bromophenyl)aminium hexachloroantimonate; In acetonitrile; at 20 ℃; Further byproducts given;

DOI:10.1039/c39850001088

Reference yield:

1,3-dioxole (288-53-9) → exo-bis-methylendioxy-cyclobutan (69956-59-8,70004-63-6,113428-72-1) + syn-dimeres-Dioxol (69956-59-8,70004-63-6,113428-72-1) + (1R,2R,6S,7S)-3,5-Dioxa-tricyclo[5.2.2.02,6]undec-8-ene + (1S,2R,6S,7R)-3,5-Dioxa-tricyclo[5.2.2.02,6]undec-8-ene

Guidance literature:

With 1,3-dioxole; tris-(4-bromophenyl)aminium hexachloroantimonate; In acetonitrile; at 20 ℃; Further byproducts given;

DOI:10.1039/c39850001088

Reference yield:

1,3-dioxole (288-53-9) + cyclohexa-1,3-diene (1165952-91-9) → exo-bis-methylendioxy-cyclobutan (69956-59-8,70004-63-6,113428-72-1) + syn-dimeres-Dioxol (69956-59-8,70004-63-6,113428-72-1) + (1R,2R,6S,7S)-3,5-Dioxa-tricyclo[5.2.2.02,6]undec-8-ene + (1S,2R,6S,7R)-3,5-Dioxa-tricyclo[5.2.2.02,6]undec-8-ene

Guidance literature:

tris-(4-bromophenyl)aminium hexachloroantimonate; In acetonitrile; at 20 ℃; Further byproducts given;

DOI:10.1039/c39850001088

upstream raw materials:

1,3-dioxole

cyclohexa-1,3-diene

benzonitrile

methoxybenzene