TERT-BUTYL 5-CHLORO-3-FORMYL-1H-INDOLE-1-CARBOXYLATE

Base Information

Chemical Name:TERT-BUTYL 5-CHLORO-3-FORMYL-1H-INDOLE-1-CARBOXYLATE
CAS No.:314248-57-2
Molecular Formula:C14H14ClNO3
Molecular Weight:279.723
Hs Code.:
Mol file:314248-57-2.mol

Synonyms:TERT-BUTYL 5-CHLORO-3-FORMYL-1H-INDOLE-1-CARBOXYLATE;1H-INDOLE-1-CARBOXYLIC ACID, 5-CHLORO-3-FORMYL-, 1,1-DIMETHYLETHYL ESTER

Suppliers and Price of TERT-BUTYL 5-CHLORO-3-FORMYL-1H-INDOLE-1-CARBOXYLATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
1H-INDOLE-1-CARBOXYLICACID,5-CHLORO-3-FORMYL-,1,1-DIMETHYLETHYLESTER 95
5g
$ 1925.00

Total 2 raw suppliers

Chemical Property of TERT-BUTYL 5-CHLORO-3-FORMYL-1H-INDOLE-1-CARBOXYLATE

Chemical Property:

PSA：48.30000
LogP:3.89040

Purity/Quality:

99% ^*data from raw suppliers

1H-INDOLE-1-CARBOXYLICACID,5-CHLORO-3-FORMYL-,1,1-DIMETHYLETHYLESTER 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of TERT-BUTYL 5-CHLORO-3-FORMYL-1H-INDOLE-1-CARBOXYLATE

There total 2 articles about TERT-BUTYL 5-CHLORO-3-FORMYL-1H-INDOLE-1-CARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 827-01-0
5-chloro-1H-indole-3-carboxaldehyde

: 24424-99-5
di-tert-butyl dicarbonate

: 314248-57-2
5-chloro-3-formyl-indole-1-carboxylic acid tert-butyl ester

Guidance literature:: With potassium carbonate; In tetrahydrofuran; for 19h;

Reference yield:

: 17422-32-1
5-chloro-1H-indole

: 314248-57-2
5-chloro-3-formyl-indole-1-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 2 h / 0 - 20 °C / Inert atmosphere

2: dmap / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

With dmap; trichlorophosphate; In tetrahydrofuran;
DOI:10.1002/anie.202102416