3-KETOFUSIDIC ACID

Base Information

• Chemical Name: 3-KETOFUSIDIC ACID
• CAS No.: 4680-37-9
• Molecular Formula: C31H46O6
• Molecular Weight: 514.703

Synonyms:3-KETOFUSIDIC ACID;(4α,8α,9β,11α,13α,14β,16β,17Z)-;Fusidic Acid EP impurityG

Chemical Property of 3-KETOFUSIDIC ACID

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 193-195 °C(Solv: ethyl ether (60-29-7); hexane (110-54-3))
• Boiling Point: 634.258°C at 760 mmHg
• PKA: 4.10±0.41(Predicted)
• Flash Point: 197.912°C
• PSA: 100.90000
• Density: 1.164g/cm³
• LogP: 5.87430
• Storage Temp.: Refrigerator
• Solubility.: Chloroform (Slightly), Methanol (Slightly)

Purity/Quality:

99%, ^*data from raw suppliers

3-KetoFusidicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 3-Keto Fusidic Acid (Fusidic Acid EP Impurity G) is a metabolite of Fusidic Acid.

Technology Process of 3-KETOFUSIDIC ACID

There total 2 articles about 3-KETOFUSIDIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

fusidine (3482-49-3,4680-36-8,6990-06-3,19030-42-3,107380-53-0) → 3-ketofusidic acid (4680-37-9)

Guidance literature:

With Jones reagent; In acetone; at 0 ℃;

DOI:10.1021/acsinfecdis.0c00869

Reference yield:

→ 3-Ketofusidinsaeure (4680-37-9,13000-32-3)

Guidance literature:

aus Fusidium coccineum;

DOI:10.1016/S0040-4020(01)93759-7

Reference yield: 51.0%

3-ketofusidic acid (4680-37-9) + O-benzylhydoxylamine hydrochloride (2687-43-6) → 3-benzyloxyiminofusidic acid

Guidance literature:

With ammonium acetate; In ethanol; at 80 ℃; for 0.333333h; Sealed tube; Microwave irradiation;

DOI:10.1016/j.bmc.2020.115530

upstream raw materials:

fusidine

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