2-AMINO-5,5,7,7-TETRAMETHYL-4,5,6,7-TETRAHYDRO-THIENO[2,3-C]PYRIDINE-3-CARBOXYLIC ACID ETHYL ESTER

Base Information

• Chemical Name: 2-AMINO-5,5,7,7-TETRAMETHYL-4,5,6,7-TETRAHYDRO-THIENO[2,3-C]PYRIDINE-3-CARBOXYLIC ACID ETHYL ESTER
• CAS No.: 133894-40-3
• Molecular Formula: C14H22N2O2S
• Molecular Weight: 282.407
• Mol file: 133894-40-3.mol

Synonyms:2-AMINO-5,5,7,7-TETRAMETHYL-4,5,6,7-TETRAHYDRO-THIENO[2,3-C]PYRIDINE-3-CARBOXYLIC ACID ETHYL ESTER;AKOS BBS-00006491;ETHYL 2-AMINO-5,5,7,7-TETRAMETHYL-4,5,6,7-TETRAHYDROTHIENO[2,3-C]PYRIDINE-3-CARBOXYLATE

Chemical Property of 2-AMINO-5,5,7,7-TETRAMETHYL-4,5,6,7-TETRAHYDRO-THIENO[2,3-C]PYRIDINE-3-CARBOXYLIC ACID ETHYL ESTER

Chemical Property:

• PSA: 92.59000
• LogP: 3.57640

Purity/Quality:

97% ^*data from raw suppliers

2-Amino-5,5,7,7-tetramethyl-4,5,6,7-tetrahydro-thieno[2,3-c]pyridine-3-carboxylicAcidEthylEster ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-AMINO-5,5,7,7-TETRAMETHYL-4,5,6,7-TETRAHYDRO-THIENO[2,3-C]PYRIDINE-3-CARBOXYLIC ACID ETHYL ESTER

There total 2 articles about 2-AMINO-5,5,7,7-TETRAMETHYL-4,5,6,7-TETRAHYDRO-THIENO[2,3-C]PYRIDINE-3-CARBOXYLIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2,6,6-Tetramethyl-4-piperidone (826-36-8) + ethyl 2-cyanoacetate (105-56-6) → 2-Amino-5,5,7,7-tetramethyl-4,5,6,7-tetrahydro-thieno[2,3-c]pyridine-3-carboxylic acid ethyl ester (133894-40-3)

Guidance literature:

With sulfur; diethylamine; In ethanol; Heating;

DOI:10.3390/molecules23071626

Reference yield:

→ 2-Amino-5,5,7,7-tetramethyl-4,5,6,7-tetrahydro-thieno[2,3-c]pyridine-3-carboxylic acid ethyl ester (133894-40-3)

Guidance literature:

Reference yield:

2-Amino-5,5,7,7-tetramethyl-4,5,6,7-tetrahydro-thieno[2,3-c]pyridine-3-carboxylic acid ethyl ester (133894-40-3) + 5-chloro-2-trifluoromethylbenzoic acid chloride (320-84-3) → C22H24ClF3N2O3S

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 22 ℃;

DOI:10.3390/molecules23071626

upstream raw materials:

2,2,6,6-Tetramethyl-4-piperidone

ethyl 2-cyanoacetate

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