Benzenepropanamine, 4-amino- (9CI)

Base Information

• Chemical Name: Benzenepropanamine, 4-amino- (9CI)
• CAS No.: 61798-01-4
• Molecular Formula: C9H14N2
• Molecular Weight: 150.224
• Hs Code.: 2921590090
• Mol file: 61798-01-4.mol

Synonyms:Benzenepropanamine, 4-amino- (9CI);4-AMino-benzenepropanaMine

Chemical Property of Benzenepropanamine, 4-amino- (9CI)

Chemical Property:

• Vapor Pressure: 0.00219mmHg at 25°C
• Boiling Point: 289.5°C at 760 mmHg
• Flash Point: 152.3°C
• PSA: 52.04000
• Density: 1.038g/cm³
• LogP: 2.44160

Purity/Quality:

97% ^*data from raw suppliers

4-(3-Aminopropyl)aniline 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenepropanamine, 4-amino- (9CI)

There total 7 articles about Benzenepropanamine, 4-amino- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(4-nitrophenyl)propanenitrile (53563-09-0) → 4-(3-aminopropyl)aniline (61798-01-4)

Guidance literature:

With methanol; platinum; at 35 ℃; under 3677.5 Torr; Hydrogenation_.nachfolgende Hydrierung an Raney-Nickel in methanol.NH₃ bei 55-70grad unter 40-60 at;

DOI:10.1039/jr9570002706

Reference yield:

3-(4-nitrophenyl)propan-1-amine (80258-61-3) → 4-(3-aminopropyl)aniline (61798-01-4)

Guidance literature:

With hydrogen; nickel; In acetic acid;

DOI:10.1021/jm00337a017

Reference yield:

N-[3-(4-nitrophenyl)propyl]-phthalimide (93324-23-3) → 4-(3-aminopropyl)aniline (61798-01-4)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) N₂H₄*H₂O, MeOH, (ii) aq. HCl

2: H₂ / Raney-Ni / acetic acid

With hydrogen; nickel; In acetic acid;

DOI:10.1021/jm00337a017

upstream raw materials:

3-(4-nitrophenyl)propanenitrile

(E)-4-nitrocinnamonitrile

1-nitro-2-(4-nitrobenzyl)ethane

3-(4-nitrophenyl)propan-1-amine

Downstream raw materials:

4-(3-isocyanato-propyl)-phenyl isocyanate

tri-N-ethyl-4-(3-triethylammonio-propyl)-anilinium; diiodide

tri-N-methyl-4-(3-trimethylammonio-propyl)-anilinium; diiodide

Undec-10-enoic acid [4-(3-undec-10-enoylamino-propyl)-phenyl]-amide