1-nitro-2-(4-nitrobenzyl)ethane

Base Information

Chemical Name:1-nitro-2-(4-nitrobenzyl)ethane
CAS No.:748814-11-1
Molecular Formula:C₉H₁₀N₂O₄
Molecular Weight:210.189
Hs Code.:

Synonyms:1-nitro-2-(4-nitrobenzyl)ethane

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Chemical Property of 1-nitro-2-(4-nitrobenzyl)ethane

Chemical Property:

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Technology Process of 1-nitro-2-(4-nitrobenzyl)ethane

There total 2 articles about 1-nitro-2-(4-nitrobenzyl)ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22818-69-5
(3-nitropropyl)benzene

: 748814-11-1
1-nitro-2-(4-nitrobenzyl)ethane

Guidance literature:: With nitric acid; at -20 - -15 ℃;
DOI:10.1021/ja01211a005

Reference yield:

: 22818-69-5
(3-nitropropyl)benzene

: 7697-37-2,78989-43-2
nitric acid

: 748814-11-1
1-nitro-2-(4-nitrobenzyl)ethane

Guidance literature:: at -20 - -15 ℃;
DOI:10.1021/ja01211a005

Reference yield: 35.6%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: copper nitrate hemi(pentahydrate)

: 1,9-diamino-3,7-diazacyclononane

: 748814-11-1
1-nitro-2-(4-nitrobenzyl)ethane

: 230621-55-3
[6-nitro-6-(4-nitrobenzyl)-1,4,8,11-tetraazacyclotetradecane]copper(II) nitrate hydrate

Guidance literature:: With Et₃N; In methanol; addn. of excess 40% aq. HCHO, Et3N and stoich. amt. nitroderivative to mixt. of equimolar amts. tetramine and Cu-salt, stirring and refluxing for 2.5 h; crystn. (room temp., overnight), recrystn. (MeOH); further crop from filtrate on prolonged standing; elem. anal.;
DOI:10.1016/S0020-1693(99)00031-6