(4S,5R)-ethyl 5-((R)-2,2-diMethyl-1,3-dioxolan-4-yl)-4-Methyl-1,3,2-dioxathiolane-4-carboxylate 2,2-dioxide

Base Information Edit

Chemical Name:(4S,5R)-ethyl 5-((R)-2,2-diMethyl-1,3-dioxolan-4-yl)-4-Methyl-1,3,2-dioxathiolane-4-carboxylate 2,2-dioxide
CAS No.:879551-01-6
Molecular Formula:C11H18O8S
Molecular Weight:310.325
Hs Code.:
Mol file:879551-01-6.mol

Synonyms:(4S,5R)-ethyl 5-((R)-2,2-diMethyl-1,3-dioxolan-4-yl)-4-Methyl-1,3,2-dioxathiolane-4-carboxylate 2,2-dioxide

Chemical Property of (4S,5R)-ethyl 5-((R)-2,2-diMethyl-1,3-dioxolan-4-yl)-4-Methyl-1,3,2-dioxathiolane-4-carboxylate 2,2-dioxide Edit

Chemical Property:

Purity/Quality:: ≥95% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Marketing and Price of (4S,5R)-ethyl 5-((R)-2,2-diMethyl-1,3-dioxolan-4-yl)-4-Methyl-1,3,2-dioxathiolane-4-carboxylate 2,2-dioxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Technology Process of (4S,5R)-ethyl 5-((R)-2,2-diMethyl-1,3-dioxolan-4-yl)-4-Methyl-1,3,2-dioxathiolane-4-carboxylate 2,2-dioxide

There total 6 articles about (4S,5R)-ethyl 5-((R)-2,2-diMethyl-1,3-dioxolan-4-yl)-4-Methyl-1,3,2-dioxathiolane-4-carboxylate 2,2-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93%

: 93635-76-8,1946820-88-7
(2S,3R)-3-[(4R)-2,2-dimethyl-[1,3]dioxolane-4-yl]-2,3-dihydroxy-2-methylpropionic acid ethyl ester

: 879551-01-6
(4S,5R)-ethyl-5-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-4-meth-yl-1,3,2-dioxathiolane-4-carboxylate 2,2-dioxide

Guidance literature:: (2S,3R)-3-[(4R)-2,2-dimethyl-[1,3]dioxolane-4-yl]-2,3-dihydroxy-2-methylpropionic acid ethyl ester; With thionyl chloride; In tetrachloromethane; acetonitrile; at 0 ℃; for 0.166667h;

With sodium periodate; triethylamine; In tetrachloromethane; water; acetonitrile; at 20 ℃; for 0.333333h; Reagent/catalyst;

Reference yield:

: 1020063-91-5
C₁₁H₁₈O₇S

: 879551-01-6
(4S,5R)-ethyl-5-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-4-meth-yl-1,3,2-dioxathiolane-4-carboxylate 2,2-dioxide

Guidance literature:: With sodium periodate; ruthenium trichloride; In tetrachloromethane; water; acetonitrile; at 20 ℃; for 0.166667h;

Reference yield:

: 21382-82-1
(carbethoxyethylidene)triphenylphosphorane

: 879551-01-6
(4S,5R)-ethyl-5-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-4-meth-yl-1,3,2-dioxathiolane-4-carboxylate 2,2-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 4.5 h / 0 - 5 °C / Large scale

2: sodium hydrogencarbonate; ethylene glycol; potassium permanganate / water; acetone / 3 h / -10 °C / Large scale

3: triethylamine; thionyl chloride / dichloromethane / 4 h / 25 °C / Large scale

With potassium permanganate; thionyl chloride; sodium hydrogencarbonate; ethylene glycol; triethylamine; In dichloromethane; water; acetone;