2-(diethylaMino)-6-Methylisonicotinic acid hcl

Base Information

Chemical Name:2-(diethylaMino)-6-Methylisonicotinic acid hcl
CAS No.:1062668-88-5
Molecular Formula:C11H17ClN2O2
Molecular Weight:244.721
Hs Code.:

Synonyms:2-(diethylaMino)-6-Methylisonicotinic acid hcl

Suppliers and Price of 2-(diethylaMino)-6-Methylisonicotinic acid hcl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(diethylaMino)-6-Methylisonicotinic acid hcl

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(diethylaMino)-6-Methylisonicotinic acid hcl

There total 1 articles about 2-(diethylaMino)-6-Methylisonicotinic acid hcl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5398-44-7
2,6-dichloropyridine-4-carboxylic acid

: 1062668-88-5
2-(diethylamino)-6-methylisonicotinic acid hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 28 h / 80 °C

2: 7 h / 100 °C

3: Pd(dppf) / 1,4-dioxane / 18 h / 75 °C

4: hydrogenchloride / water / 72 h / 80 °C

With hydrogenchloride; sulfuric acid; Pd(dppf); In 1,4-dioxane; water;

Reference yield: 61.0%

: 910635-33-5
3-ethyl-N,4-dihydroxy-5-methylbenzimidamide

: 1062668-88-5
2-(diethylamino)-6-methylisonicotinic acid hydrochloride

: 1062669-89-9
4-(5-(2-(diethylamino)-6-methylpyridin-4-yl)-1,2,4-oxadiazol-3-yl)-2-ethyl-6-methylphenol

Guidance literature:: 3-ethyl-N,4-dihydroxy-5-methylbenzimidamide; 2-(diethylamino)-6-methylisonicotinic acid hydrochloride; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; Inert atmosphere;

In 1,4-dioxane; at 80 - 100 ℃; Reagent/catalyst; Inert atmosphere;
DOI:10.1021/jm4014696

Reference yield:

: 1062668-88-5
2-(diethylamino)-6-methylisonicotinic acid hydrochloride

: 910635-33-5
3-ethyl-N,4-dihydroxy-5-methylbenzimidamide

: C₂₁H₂₈N₄O₃

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; at -5 - 0 ℃; for 2h;
DOI:10.1021/op200326s