7-Chloro-4,6-dimethoxy-6'-methylspiro[benzofuran-2(3H),1'-cyclohexane]-3,4'-dione

Base Information

Chemical Name:7-Chloro-4,6-dimethoxy-6'-methylspiro[benzofuran-2(3H),1'-cyclohexane]-3,4'-dione
CAS No.:17793-65-6
Molecular Formula:C₁₆H₁₇ClO₅
Molecular Weight:324.761
Hs Code.:
Mol file:17793-65-6.mol

Synonyms:7-Chloro-4,6-dimethoxy-6'-methylspiro[benzofuran-2(3H),1'-cyclohexane]-3,4'-dione

Suppliers and Price of 7-Chloro-4,6-dimethoxy-6'-methylspiro[benzofuran-2(3H),1'-cyclohexane]-3,4'-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-Chloro-4,6-dimethoxy-6'-methylspiro[benzofuran-2(3H),1'-cyclohexane]-3,4'-dione

Chemical Property:

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Technology Process of 7-Chloro-4,6-dimethoxy-6'-methylspiro[benzofuran-2(3H),1'-cyclohexane]-3,4'-dione

There total 25 articles about 7-Chloro-4,6-dimethoxy-6'-methylspiro[benzofuran-2(3H),1'-cyclohexane]-3,4'-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126-07-8,469-49-8,1588-01-8,2884-22-2,6915-11-3,67890-77-1,78739-00-1
(+)-epigriseofulvin

: 17793-65-6,17794-02-4,86594-42-5
(-)-2'-demethoxy-2',3'-dihydroepigriseofulvin

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / 5percent palladium on charcoal / ethyl acetate / 2 h / Ambient temperature

2: 2N sulfuric acid / ethanol; H₂O / 6 h / Heating

3: hydrogen / 5percent palladium on charcoal / ethyl acetate / 4 h / Ambient temperature

With sulfuric acid; hydrogen; palladium on activated charcoal; In ethanol; water; ethyl acetate;
DOI:10.1248/cpb.31.934