1-Chloro-3-iodo-5-methylbenzene

Base Information

Chemical Name:1-Chloro-3-iodo-5-methylbenzene
CAS No.:116632-43-0
Molecular Formula:C7H6ClI
Molecular Weight:252.482
Hs Code.:
DSSTox Substance ID:DTXSID901303705
Mol file:116632-43-0.mol

Synonyms:1-chloro-3-iodo-5-methylbenzene;3-Chloro-5-iodotoluene;116632-43-0;1-Chloro-3-iodo-5-methyl-benzene;SCHEMBL13310150;DTXSID901303705;MFCD13185456;AS-36916;CS-0153256;FT-0727031;EN300-3542897

Suppliers and Price of 1-Chloro-3-iodo-5-methylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-Chloro-3-iodo-5-methylbenzene
10mg
$ 45.00

Chemcia Scientific
1-Chloro-3-iodo-5-methyl-benzene ＞95%
5 G
$ 1050.00

Ambeed
1-Chloro-3-iodo-5-methylbenzene 95%
5g
$ 465.00

Ambeed
1-Chloro-3-iodo-5-methylbenzene 95%
1g
$ 168.00

Ambeed
1-Chloro-3-iodo-5-methylbenzene 95%
250mg
$ 98.00

Alichem
3-Chloro-5-iodotoluene
1g
$ 1445.30

Total 6 raw suppliers

Chemical Property of 1-Chloro-3-iodo-5-methylbenzene

Chemical Property:

Melting Point:0 °C
Boiling Point:138-140 °C(Press: 26 Torr)
PSA：0.00000
Density:1.806±0.06 g/cm3(Predicted)
LogP:3.25300
Storage Temp.:2-8°C(protect from light)
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:251.92028
Heavy Atom Count:9
Complexity:94.9

Purity/Quality:

99% ^*data from raw suppliers

1-Chloro-3-iodo-5-methylbenzene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC(=C1)I)Cl

Technology Process of 1-Chloro-3-iodo-5-methylbenzene

There total 5 articles about 1-Chloro-3-iodo-5-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 502630-89-9
2-(3-chloro-5-methylphenyl)-4,4,5,5-tetra methyl-1,3,2-dioxaborolane

: 116632-43-0
1-chloro-3-iodo-5-methylbenzene

Guidance literature:: With copper(l) iodide; 1,10-Phenanthroline; potassium iodide; In methanol; water; at 80 ℃; for 1h; High pressure;
DOI:10.1021/ol303164h

Reference yield:

: 108-41-8
1-chloro-3-methylbenzene

: 116632-43-0
1-chloro-3-iodo-5-methylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4′-di-(tert-butyl)-2,2′-bipyridyl / tetrahydrofuran / 24 h / 80 °C / High pressure; Inert atmosphere

2: 1,10-Phenanthroline; copper(l) iodide; potassium iodide / methanol; water / 1 h / 80 °C / High pressure

With copper(l) iodide; 1,10-Phenanthroline; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4′-di-(tert-butyl)-2,2′-bipyridyl; potassium iodide; In tetrahydrofuran; methanol; water;
DOI:10.1021/ol303164h