3-Pyridinemethanol stearate

Base Information

• Chemical Name: 3-Pyridinemethanol stearate
• CAS No.: 82120-89-6
• Molecular Formula: C₂₄H₄₁NO₂
• Molecular Weight: 375.595
• Mol file: 82120-89-6.mol

Synonyms:3-Pyridinemethanol stearate;Octadecanoic acid (3-pyridyl)methyl ester;Stearic acid picolinyl ester;β-Picolinyl stearate

Chemical Property of 3-Pyridinemethanol stearate

Chemical Property:

• PSA: 39.19000
• LogP: 7.38630

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Pyridinemethanol stearate

There total 3 articles about 3-Pyridinemethanol stearate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.03%

3-hydroxymethylpyridin (100-55-0) + stearic acid (57-11-4) → 3-picolinyl stearate (82120-89-6)

Guidance literature:

stearic acid; With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 0.25h;

3-hydroxymethylpyridin; In dichloromethane; at 20 ℃; for 60h; Further stages.;

DOI:10.1039/b706657k

Reference yield:

stearic acid (57-11-4) → 3-picolinyl stearate (82120-89-6)

Guidance literature:

Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane / 0.08 h / 65 °C

2: acetonitrile / 0.08 h / 20 °C

With oxalyl dichloride; In dichloromethane; acetonitrile;

DOI:10.1021/ac103093w

Reference yield:

3-hydroxymethylpyridin (100-55-0) + Stearoyl chloride (112-76-5) → 3-picolinyl stearate (82120-89-6)

Guidance literature:

In acetonitrile; at 20 ℃; for 0.0833333h;

DOI:10.1021/ac103093w

upstream raw materials:

3-hydroxymethylpyridin

stearic acid

Stearoyl chloride