Diethyl(vinyl)phosphine

Base Information

Chemical Name:Diethyl(vinyl)phosphine
CAS No.:13652-21-6
Molecular Formula:C6H13P
Molecular Weight:116.14
Hs Code.:
Mol file:13652-21-6.mol

Synonyms:Diethyl(vinyl)phosphine

Suppliers and Price of Diethyl(vinyl)phosphine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Diethyl(vinyl)phosphine

Chemical Property:

Boiling Point:125 °C(Press: 744 Torr)
PSA：13.59000
LogP:2.65160

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Diethyl(vinyl)phosphine

There total 2 articles about Diethyl(vinyl)phosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 686-69-1
diethylchlorophosphine

: 1826-67-1
vinyl magnesium bromide

: 13652-21-6
diethylvinyl phosphine

Guidance literature:: In tetrahydrofuran; for 24h;
DOI:10.1021/ja00311a034

Reference yield:

: 13652-21-6
diethylvinyl phosphine

Guidance literature:: Chlor-diethyl-phosphin (in Dibutylether), Vinyl-Na;

Reference yield: 94.8%

: 86421-54-7,86495-69-4
trans, trans, trans-dichlorodicarbonylbis(1-phenyl-3,4-dimethylphosphole)ruthenium(II)

: 13652-21-6
diethylvinyl phosphine

: 123099-52-5
mer-trans-dichlorocarbonyl(1-phenyl-3,4-dimethylphosphole)(2-(diethylphosphino)-5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-ene)ruthenium(II)

Guidance literature:: In dichloromethane; under N2; soln. stirred for ca. 24 h at room temp.; filtration, concn., addn. of ethanol, ppt. washed with ethanol, anhydrous Et2O, vacuum-dried overnight, elem. anal.;
DOI:10.1021/ic00321a019