Technology Process of 1-Iodo-5-nitronaphthalene
There total 5 articles about 1-Iodo-5-nitronaphthalene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
5-nitro-[1]naphthylamine;
With
sulfuric acid; sodium nitrite;
In
acetic acid;
at 0 ℃;
for 0.5h;
With
urea; potassium iodide;
In
water; acetic acid;
for 8h;
Cooling with ice;
DOI:10.1039/c5tc04236d
- Guidance literature:
-
With
reagent "I(1+)";
In
sulfuric acid;
at 0 ℃;
for 1.5h;
DOI:10.1007/BF02495292
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 54 percent / NH4Cl; 28percent aq. NH3; Na2S / H2O / 4 h / 80 - 85 °C
2: 76 percent / NaNO2; KI; urea / H2SO4; acetic acid; H2O / 0 °C
With
sodium sulfide; ammonium chloride; urea; potassium iodide; sodium nitrite;
In
sulfuric acid; water; acetic acid;
DOI:10.1021/jo0203589